Liu Xin, Yu Wenchao, Che Hanlin, Zhang Jugan, Zhu Jiahao, Jiang Qingwei, Zhang Chi, Wang Maoqiu
School of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, China.
Central Iron & Steel Research Institute Company Limited, Beijing 100081, China.
Materials (Basel). 2024 Nov 29;17(23):5855. doi: 10.3390/ma17235855.
To avoid grain coarsening resulting from high-temperature carburizing, the effects of cyclic quenching and tempering on the microstructure and mechanical properties of 18CrNiMo7-6 gear steel were investigated. Three groups of samples were compared, which went through 0/1/3 times of quenching-tempering cycles after initial pseudo-carburizing. The variations in grain size, hardness, tensile strength, and toughness were systematically assessed using a series of experimental techniques. The experimental results indicate that the austenite grain size decreases from 14.8 μm to 5.0 μm as the number of cycles increases, accompanied by improved grain uniformity, which is beneficial to fine-grain strengthening mechanisms. During the phase transition, defects in the original martensite structure are transferred to the newly formed austenite, with the energy stored during the martensitic-to-austenitic transformation driving the grain refinement process. However, after several cycles of quenching and tempering, the release of some residual stresses and dislocations reduces the driving force for recrystallization, limiting further grain refinement. Although the strength decreased slightly after three cycles due to a reduction in dislocation density, toughness increased to a maximum of 172 J/cm, primarily due to the enhancement of grain refinement and grain boundary density, which effectively hindered crack propagation. This study confirms the efficacy of cyclic heat treatment in refining grain structure and improving both strength and toughness, thereby contributing valuable insights to the research and development of high-performance gear steels.
为避免高温渗碳导致晶粒粗大,研究了循环淬火和回火对18CrNiMo7-6齿轮钢组织和力学性能的影响。比较了三组样品,它们在初始伪渗碳后分别经历了0/1/3次淬火-回火循环。使用一系列实验技术系统地评估了晶粒尺寸、硬度、抗拉强度和韧性的变化。实验结果表明,随着循环次数的增加,奥氏体晶粒尺寸从14.8μm减小到5.0μm,同时晶粒均匀性得到改善,这有利于细晶强化机制。在相变过程中,原始马氏体组织中的缺陷转移到新形成的奥氏体中,马氏体向奥氏体转变过程中储存的能量驱动晶粒细化过程。然而,经过几次淬火和回火循环后,一些残余应力和位错的释放降低了再结晶驱动力,限制了进一步的晶粒细化。尽管由于位错密度降低,三次循环后强度略有下降,但韧性增加到最大值172J/cm,这主要是由于晶粒细化和晶界密度的提高有效地阻碍了裂纹扩展。本研究证实了循环热处理在细化晶粒组织以及提高强度和韧性方面的有效性,从而为高性能齿轮钢的研发提供了有价值的见解。