Luo Yilian, Jiang Liangwei, Qin Libing, Luo Qiang, Connolly David P, Wang Tengfei
School of Civil Engineering, Southwest Jiaotong University, Chengdu 610031, China.
Key Laboratory of High-Speed Railway Engineering, Ministry of Education, Southwest Jiaotong University, Chengdu 610031, China.
Materials (Basel). 2024 Dec 3;17(23):5915. doi: 10.3390/ma17235915.
The Ethylene Diamine Tetra-acetic Acid (EDTA) titration test is widely used for determining cement content, but its reliability is influenced by the hydration process of cement, which is affected by factors such as water content and hydration time. Despite their importance, these factors have received limited attention in existing research. This study explores the relationships between the volume of titrant required for stabilization, cement content, water content, and hydration time. Using a regression orthogonal test, the primary and secondary relationships, as well as the interdependencies among these factors, are analyzed. Results reveal a negative linear relationship between the titrant volume and both water content and hydration time. Cement content, water content, and hydration time are identified as the most significant factors, with minimal interdependencies observed. Within the test parameters, calculated values exhibit an error margin below 2.4%. Deviations of 2.9% in water content and 86 min in hydration time correspond to an approximate 0.5% change in cement content. These findings offer valuable insights for optimizing cement content detection in Controlled Low-Strength Material (CLSM) mixes, promoting more sustainable construction practices.
乙二胺四乙酸(EDTA)滴定试验被广泛用于测定水泥含量,但其可靠性受水泥水化过程的影响,而水泥水化过程又受含水量和水化时间等因素影响。尽管这些因素很重要,但在现有研究中受到的关注有限。本研究探讨了稳定所需滴定剂体积、水泥含量、含水量和水化时间之间的关系。采用回归正交试验,分析了这些因素之间的主次关系以及相互依存关系。结果表明,滴定剂体积与含水量和水化时间均呈负线性关系。水泥含量、含水量和水化时间被确定为最显著的因素,相互依存关系最小。在试验参数范围内,计算值的误差幅度低于2.4%。含水量偏差2.9%和水化时间偏差86分钟对应水泥含量约0.5%的变化。这些发现为优化可控低强度材料(CLSM)混合料中水泥含量检测提供了有价值的见解,有助于推动更可持续的建筑实践。