Niu Fengjiao, Ma Zibo, Hao Yixuan, Guo Yajie, Cao Peng
School of Materials Science and Engineering, Chang'an University, Shaanxi 710064, China; Modern Engineering Training Center, Chang'an University, Shaanxi 710064, China.
School of Materials Science and Engineering, Chang'an University, Shaanxi 710064, China.
Micron. 2025 Mar;190:103779. doi: 10.1016/j.micron.2024.103779. Epub 2024 Dec 25.
This study investigates the effect of pre-deformation by cold rolling after solution annealing on the microstructure and properties of the fine-grained Al-Li alloy 2A97. Electron backscatter diffraction (EBSD), X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used to characterize grain boundaries, dislocations, precipitates and calculate their contribution to strength. It is found that the changes in precipitation behavior predominantly account for the enhanced tensile properties observed in the deformed alloys, where yield and tensile strengths are increased by 85 MPa and 63 MPa, respectively. The peak-aged samples without pre-deformation are mainly strengthened by the T phase, δ'/θ'/δ' composite and σ phase. In contrast, deformation of 10 % prior to aging facilitates the precipitation of the T and lath-like S phases while concurrently inhibiting the precipitation of the σ phase and δ'/θ'/δ' composite phases. In addition, for fine-grained alloys, low-angle grain boundaries induce the precipitation of the finer T phase compared to the T phase located inside the grain, which contributes to the good performance of 2A97 alloy.
本研究调查了固溶退火后冷轧预变形对细晶Al-Li合金2A97微观结构和性能的影响。采用电子背散射衍射(EBSD)、X射线衍射(XRD)和透射电子显微镜(TEM)对晶界、位错、析出相进行表征,并计算它们对强度的贡献。结果发现,析出行为的变化是变形合金拉伸性能增强的主要原因,其中屈服强度和抗拉强度分别提高了85MPa和63MPa。未经预变形的峰值时效样品主要由T相、δ'/θ'/δ'复合体和σ相强化。相比之下,时效前10%的变形促进了T相和板条状S相的析出,同时抑制了σ相和δ'/θ'/δ'复合相的析出。此外,对于细晶合金,与晶粒内部的T相相比,低角度晶界会诱导更细小的T相析出,这有助于2A97合金具有良好的性能。