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壳聚糖与聚乙烯醇活性薄膜的制备与表征:掺入几内亚蒲桃植物提取物作为活性包装材料

Preparation and characterization of chitosan and polyvinyl alcohol active film incorporated with Syzygium guineense plant extract as active packaging materials.

作者信息

Khan Jehangir, Alam Shah, Nazir Afaq, Tian Dingwei, Abbas Muhammad Qamar, Du Zhenxia

机构信息

College of Chemistry, Beijing University of Chemical Technology, Beijing 100029, People's Republic of China.

Department of Entomology, PMAS-Arid Agriculture University, Rawalpindi, Pakistan.

出版信息

Int J Biol Macromol. 2025 Apr;299:140155. doi: 10.1016/j.ijbiomac.2025.140155. Epub 2025 Jan 21.

Abstract

The advancement of active packaging for food conservation has attracted considerable interest over time. In the present study, we aims to create and examine active films composed of chitosan (CS), poly(vinyl alcohol) (PVA), and syzygium guineense plant extract (SYZ) for potential use in food preservation. We examined the impact of ethanol extracts from the SYZ plant on the films' tensile strength, physical, antibacterial, and anti-oxidant properties. Scanning electron microscopy showed that the fabricated films have an even, uniform exterior morphology as well as superior UV-blocking capabilities. FTIR and X-ray diffraction analyses indicated that SYZ interacts with the CS/PVA blend through H-bonding. The addition of SYZ plant extract significantly increases the tensile strength of the films, reaching up to 88.61 ± 3.17 MPa. Furthermore, the water vapor transmission rate decreases to (0.34 ± 0.35 g·smPa) × 10 with the inclusion of SYZ plant extracts. All fabricated films maintain in general migration rate within permissible limits (<10 mg/dm). Additionally, CS/PVA films with SYZ plant extract exhibit better anti-bacterial assay against S. aureus and E. coli. All samples containing SYZ plant extracts shows improved antioxidant activity based on DPPH and ABTS radical inhibition. These findings suggest that fabricated films with SYZ plant extract are promising for food wrapping.

摘要

随着时间的推移,用于食品保鲜的活性包装的发展引起了相当大的关注。在本研究中,我们旨在制备并检测由壳聚糖(CS)、聚乙烯醇(PVA)和几内亚番樱桃植物提取物(SYZ)组成的活性薄膜,以探讨其在食品保鲜中的潜在用途。我们研究了SYZ植物乙醇提取物对薄膜拉伸强度、物理性能、抗菌性能和抗氧化性能的影响。扫描电子显微镜显示,制备的薄膜具有均匀、一致的外观形态以及优异的紫外线阻隔能力。傅里叶变换红外光谱(FTIR)和X射线衍射分析表明,SYZ通过氢键与CS/PVA共混物相互作用。添加SYZ植物提取物显著提高了薄膜的拉伸强度,最高可达88.61±3.17MPa。此外,随着SYZ植物提取物的加入,水蒸气透过率降至(0.34±0.35g·smPa)×10。所有制备的薄膜的总体迁移率均保持在允许范围内(<10mg/dm)。此外,含有SYZ植物提取物的CS/PVA薄膜对金黄色葡萄球菌和大肠杆菌表现出更好的抗菌效果。基于二苯基苦味酰基自由基(DPPH)和2,2'-联氮-双-3-乙基苯并噻唑啉-6-磺酸(ABTS)自由基抑制,所有含有SYZ植物提取物的样品均表现出增强的抗氧化活性。这些发现表明,含有SYZ植物提取物的制备薄膜在食品包装方面具有广阔前景。

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