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不同加热和冷却持续时间下高温红砂岩的微观损伤演化及物理力学行为

Microscopic damage evolution and physical-mechanical behavior of high-temperature red sandstone under varying heating and cooling durations.

作者信息

Qin Mingze, Su Yue, Wang Xiaolan, Niu Huawu, Zhang Yifan, Zhang Dongxu, Qin Nan

机构信息

School of Mechanical and Electrical Engineering, Qingdao University of Science and Technology, Qingdao, 266061, China.

Mount Taishan Vocational and Technical College, Taian, 271000, China.

出版信息

Sci Rep. 2025 Jan 31;15(1):3942. doi: 10.1038/s41598-025-87925-5.

Abstract

The investigation into the cooling and heating duration is crucial for evaluating the aftermath of a fire incident. This study comprehensively analyzes the macroscopic and microscopic characteristics of red sandstone under high temperatures, heating, and cooling conditions, with temperatures ranging from 200 to 800 °C and heating/cooling durations ranging from 0.75 to 3 h and 0.5 to 54 h, respectively XRD and SEM techniques were employed to investigate mineral composition and microstructural changes. Multifactorial experiments explored the impact of these conditions on the rock's physical properties and assessed mechanical properties such as peak stress, peak strain, and elastic modulus. Data fitting with MATLAB was used to construct a damage constitutive model. The findings show that elevated temperatures and prolonged heating significantly alter the microstructure and composition of red sandstone, including pore formation, void development, and structural modifications. Heating induces cracking, voids, and chemical reactions, with extended exposure leading to changes in feldspar minerals (K/Ca/Na). Temperature-dependent physical properties exhibit mass loss and density decline. Mechanical properties are substantially affected, with peak stress decreasing from 40 MPa to 6.94 MPa, and variations in peak strain and elastic modulus. Thermal stress at specific temperatures notably enhances compressive strength. The newly established constitutive model has an error within 5% compared to actual experimental results.

摘要

对冷却和加热持续时间的研究对于评估火灾事故的后果至关重要。本研究全面分析了红砂岩在200至800°C的高温、加热和冷却条件下的宏观和微观特征,加热/冷却持续时间分别为0.75至3小时和0.5至54小时。采用XRD和SEM技术研究矿物成分和微观结构变化。多因素实验探讨了这些条件对岩石物理性质的影响,并评估了峰值应力、峰值应变和弹性模量等力学性能。使用MATLAB进行数据拟合以构建损伤本构模型。研究结果表明,温度升高和加热时间延长会显著改变红砂岩的微观结构和成分,包括孔隙形成、孔洞发展和结构改变。加热会引发开裂、孔洞和化学反应,长时间暴露会导致长石矿物(钾/钙/钠)发生变化。与温度相关的物理性质表现为质量损失和密度下降。力学性能受到显著影响,峰值应力从40MPa降至6.94MPa,峰值应变和弹性模量也发生变化。特定温度下的热应力显著提高了抗压强度。新建立的本构模型与实际实验结果相比误差在5%以内。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/817b/11785982/dc3c0940ecc5/41598_2025_87925_Fig1_HTML.jpg

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