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碱处理及其对芭蕉假茎纤维物理力学性能的影响——处理纤维与未处理纤维的对比研究

The alkaline treatment and its influence on the physicomechanical properties of plantain pseudostem fibers - A comparative study of treated and untreated fibers.

作者信息

Hurtado-Figueroa Oswaldo, Varum Humberto, Prieto María Isabel, Gallardo Amaya Romel J, Escamilla Alfonso Cobo

机构信息

Escuela Técnica Superior de Edificación, Universidad Politécnica de Madrid-UPM, 28040 Madrid, Spain.

Grupo de Investigación en Construcción, Geotecnia y Medio Ambiente-GIGMA, Universidad Francisco de Paula Santander Ocaña-UFPSO, 546552 Ocaña, Colombia.

出版信息

Heliyon. 2025 Jan 9;11(2):e41843. doi: 10.1016/j.heliyon.2025.e41843. eCollection 2025 Jan 30.

Abstract

Fibers were extracted from the pseudostem of the plantain of the variety Hartón, belonging to the order Zingiberales, family Musaceae, genus Musa, species Musa paradisiaca. The fibers were exposed to alkaline treatment to improve their physicomechanical properties for use as reinforcement in green composites. solutions of 4 %, 5 %, and 6 % by weight were prepared. The fibers were immersed for 2 h in each solution. Fibers were washed with acetic acid to remove residues and dried at room temperature. Weight loss and lignin, cellulose, and hemicellulose content were evaluated. FTIR, tensile, and elongation tests were performed. SEM images and EDS mapping allowed to conclude the phenomena that occurred in the treatments. The untreated fibers obtained a tensile strength of 37.23 MPa, in contrast to 104.26 MPa obtained by the fibers treated with 5 % NaOH solution. It was concluded that the partial elimination of impurities and waxes improved the mechanical behavior of the fibers by 180 %. Regarding elongation, the fibers treated with 4 % NaOH solution obtained the best result with 3.7 %. It was determined that the partial elimination of lignin favors elongation by 48 %. Excessive hemicellulose removal was found to cause fibril separation and detachment. Considerable contraction of vascular bundles occurred. Roughness in the fibers surface topography were improved.

摘要

纤维取自属于姜目、芭蕉科、芭蕉属、 paradisiaca 种的 Hartón 品种大蕉的假茎。将这些纤维进行碱处理以改善其物理机械性能,用作绿色复合材料中的增强材料。制备了重量百分比为4%、5%和6%的溶液。将纤维在每种溶液中浸泡2小时。用乙酸洗涤纤维以去除残留物,并在室温下干燥。评估了重量损失以及木质素、纤维素和半纤维素的含量。进行了傅里叶变换红外光谱(FTIR)、拉伸和伸长率测试。扫描电子显微镜(SEM)图像和能谱分析(EDS)图谱有助于推断处理过程中发生的现象。未处理的纤维获得的拉伸强度为37.23MPa,相比之下,用5%氢氧化钠溶液处理的纤维获得的拉伸强度为104.26MPa。得出的结论是,杂质和蜡的部分去除使纤维的机械性能提高了180%。关于伸长率,用4%氢氧化钠溶液处理的纤维获得了最佳结果,为3.7%。确定木质素的部分去除有利于伸长率提高48%。发现半纤维素的过度去除会导致原纤维分离和脱落。维管束出现了相当大的收缩。纤维表面形貌的粗糙度得到了改善。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6033/11783020/6e0db10a95eb/ga1.jpg

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