Diao Jiecheng, Gao Zichen, Fan Jiadong, Tong Yajun, Ren Hang, Nie Yonggan, Robinson Ian, Jiang Huaidong
Center for Transformative Science, ShanghaiTech University, Shanghai 201210, People's Republic of China.
London Centre for Nanotechnology, University College London, London WC1E 6BT, United Kingdom.
IUCrJ. 2025 Mar 1;12(Pt 2):239-244. doi: 10.1107/S2052252524012521.
We used a soft X-ray free-electron laser and the Bragg coherent diffraction imaging method to characterize the defect structure of colloidal crystals. The single-shot X-ray pulse allowed us to reach four powder rings and measured all six reflections of the hexagonal lattice. We reproduced the static shape of the 2D crystal and mapped out the 2D strain tensors inside the crystal. The observed defect structures agreed with electron microscope images of similar colloidal samples.
我们使用软X射线自由电子激光和布拉格相干衍射成像方法来表征胶体晶体的缺陷结构。单次X射线脉冲使我们能够获得四个粉末环,并测量六角晶格的所有六个反射。我们再现了二维晶体的静态形状,并绘制出了晶体内的二维应变张量。观察到的缺陷结构与类似胶体样品的电子显微镜图像相符。