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基于丙烯酸树脂颗粒的复杂裂缝地层凝胶堵漏体系的开发与性能评价

Development and Performance Evaluation of a Gel-Based Plugging System for Complex Fractured Formations Using Acrylic Resin Particles.

作者信息

Yao Lei, Quan Xiaohu, Ma Jihe, Wang Ge, Feng Qi, Jin Hui, Yang Jun

机构信息

China Oilfield Services Limited (COSL), China National Offshore Oil Corporation, Sanhe 065200, China.

Oil and Gas Resources Research Center, Ningxia University, Yinchuan 750021, China.

出版信息

Gels. 2025 Feb 24;11(3):162. doi: 10.3390/gels11030162.

Abstract

The issue of fluid loss in fractured formations presents a significant challenge in petroleum engineering, often leading to increased operational costs and construction risks. To address the limitations of traditional lost circulation materials (LCMs) in oil reservoirs with different fracture sizes, this study developed an acrylic resin gel particle with excellent thermal stability (thermal decomposition temperature up to 314 °C) and compatibility. By employing Box-Behnken design and response surface methodology, the synergistic interaction of calcium hydroxide (Ca(OH)), asbestos fibers, and cement was optimized to create a novel gel solidification plugging system that meets the requirements of fluid loss control and compressive strength improvement. Experimental results revealed that the gel-based system demonstrated exceptional performance, achieving rapid fluid loss (total fluid loss time of 18~47 s) and forming a high-strength gelled filter cake (24 h compressive strength up to 17.5 MPa). Under simulated conditions (150 °C), the gel-based system provided efficient fracture sealing, showcasing remarkable adaptability and potential for engineering applications. This study underscores the promise of acrylic resin gel particles in overcoming fluid loss challenges in complex fractured formations.

摘要

裂缝性地层中的流体损失问题在石油工程中构成了重大挑战,常常导致运营成本增加和施工风险上升。为解决传统堵漏材料(LCMs)在不同裂缝尺寸油藏中的局限性,本研究开发了一种具有优异热稳定性(热分解温度高达314°C)和相容性的丙烯酸树脂凝胶颗粒。通过采用Box-Behnken设计和响应面方法,优化了氢氧化钙(Ca(OH))、石棉纤维和水泥的协同相互作用,以创建一种满足流体损失控制和抗压强度提高要求的新型凝胶固化堵漏体系。实验结果表明,基于凝胶的体系表现出卓越性能,实现了快速流体损失(总流体损失时间为18~47秒)并形成了高强度凝胶滤饼(24小时抗压强度高达17.5MPa)。在模拟条件(150°C)下,基于凝胶的体系提供了有效的裂缝封堵,展现出显著的适应性和工程应用潜力。本研究强调了丙烯酸树脂凝胶颗粒在克服复杂裂缝性地层中流体损失挑战方面的前景。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/490f/11942553/8d8602bbb078/gels-11-00162-g001.jpg

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