Salieva Gulrukh, Kholikov Tursunali, Okmanov Rasul Ya, Matchanov Alimjon, Khodjaniyazov Khamid U, Kadirova Shakhnoza, Torambetov Batirbay
National University of Uzbekistan named after Mirzo Ulugbek 4 University St Tashkent 100174 Uzbekistan.
Tashkent Medical Academy, 2 Farabi St, Tashkent, 100109, Uzbekistan.
Acta Crystallogr E Crystallogr Commun. 2025 Mar 25;81(Pt 4):328-331. doi: 10.1107/S2056989025002440. eCollection 2025 Apr 1.
The title compound, CHNS (DAMP-DMB), was synthesized through the reaction of 2,4-di-methyl-benzyl chloride with di-amino-pyrimidine-thiol. Single-crystal X-ray diffraction analysis confirmed that the compound crystallizes in the monoclinic crystal system, space group 2/. The asymmetric unit contains a single mol-ecular entity. Structural examination revealed the presence of a dimeric arrangement consolidated by N-H⋯N hydrogen-bonding inter-actions. Additionally, Hirshfeld surface analysis indicated that H⋯H, N⋯H, C⋯H, and S⋯H contacts account for 98.9% of the total inter-molecular inter-actions to the Hirshfeld surface.
标题化合物CHNS（DAMP-DMB）通过2,4-二甲基苄基氯与二氨基嘧啶硫醇反应合成。单晶X射线衍射分析证实该化合物结晶于单斜晶系，空间群为2/。不对称单元包含一个单分子实体。结构研究表明存在由N-H⋯N氢键相互作用巩固的二聚体排列。此外，Hirshfeld表面分析表明H⋯H、N⋯H、C⋯H和S⋯H接触占与Hirshfeld表面的总分子间相互作用的98.9%。
