通过多米诺C-N偶联/氢胺化反应合成吡咯并[3,2-]嘧啶-2,4(3)-二酮
Synthesis of pyrrolo[3,2-]pyrimidine-2,4(3)-diones by domino C-N coupling/hydroamination reactions.
作者信息
Figueira de Abreu Ruben Manuel, Tiedemann Robin, Ehlers Peter, Langer Peter
机构信息
Universität Rostock, Institut für Chemie, Albert-Einstein-Str. 3a, 18059 Rostock, Germany.
Leibniz Institut für Katalyse an der Universität Rostock e. V., Albert-Einstein-Str. 29a, 18059 Rostock, Germany.
出版信息
Beilstein J Org Chem. 2025 May 22;21:1010-1017. doi: 10.3762/bjoc.21.82. eCollection 2025.
A variety of pyrrolo[3,2-]pyrimidine-2,4(3)-diones were prepared by a combination of Sonogashira reaction and subsequent cyclization by domino C-N coupling/hydroamination reaction. The optical properties (UV-vis absorption and fluorescence) depend on the substitution pattern of the compounds.
通过Sonogashira反应与随后的多米诺C-N偶联/氢胺化反应环化相结合，制备了多种吡咯并[3,2-]嘧啶-2,4(3)-二酮。光学性质（紫外-可见吸收和荧光）取决于化合物的取代模式。
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