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具有可变可持续性特征的增材制造牙科托盘材料的机械性能和粘附性能。

Mechanical and adhesive properties of additively manufactured dental tray materials with variable sustainability profiles.

作者信息

Clarkson Petra, Heenan Rachael, Liu Xiaoyun, Cameron Andrew B, Newsham-West Kathryn, Aarts John M, Choi Joanne J E

机构信息

Sir John Walsh Research Institute, Faculty of Dentistry, University of Otago, Dunedin, New Zealand.

Sir John Walsh Research Institute, Faculty of Dentistry, University of Otago, Dunedin, New Zealand; School of Medicine and Dentistry, Griffith University, Gold Coast Campus, Australia.

出版信息

J Mech Behav Biomed Mater. 2025 Oct;170:107115. doi: 10.1016/j.jmbbm.2025.107115. Epub 2025 Jun 27.

Abstract

OBJECTIVE

To assess the mechanical and adhesive properties of additively manufactured (AM) materials with variable sustainability and recyclability as alternatives to traditional light-cured acrylic resin for dental custom trays.

MATERIALS AND METHOD

Four different AM materials; a photopolymer resin tray material printed with DLP and three FDM printed polylactic acid (PLA), recycled PLA and Polyethylene Terephthalate Glycol (PETG) and a conventional light-cure acrylic resin (LC PMMA) as a control were used to construct dumbbell (tensile testing), rectangular (flexural testing) to verify suitability for custom trays (n=10/group). To evaluate bond strength, specimens were manufactured at 0, 45 and 90° printing orientation (n=10/group). Surface roughness was evaluated with confocal scanning microscopy. The three mechanical tests were completed in a universal testing machine (Instron) according to ISO 527-2 and ISO 20795-1. Results were statistically analysed with PRISM (Version 10) Software using one-way ANOVA and Kruskal-Wallis tests, with statistical significance set at p < 0.05. Confocal analysis and SEM analysis were conducted for quantitative and qualitative surface analysis.

RESULTS

For tensile and flexural strength, PLA (Recycled) and PETG showed no statistically significant difference (p > 0.05) from LC PMMA. AM materials yielded a higher bond strength than the LC PMMA material. Print orientation was found to affect the bond strength of some materials with varying surface roughness as contributing factors.

CONCLUSION

LC PMMA, PLA (Recycled), and PETG have the greatest flexural and tensile strengths. PLA (Recycled) and PETG were the highest performing AM options with regard to flexural and tensile strength for custom trays. All AM materials showed a significantly higher bond strength compared to LC PMMA. To maximise the bond strength, PLA (Recycled) should be printed at an angle of 0°, and PETG at 0 or 90°. Dental practitioners should consider the varying degrees of recyclability of materials, in addition to their mechanical properties.

摘要

目的

评估具有不同可持续性和可回收性的增材制造(AM)材料作为牙科定制托盘传统光固化丙烯酸树脂替代品的机械性能和粘附性能。

材料与方法

使用四种不同的增材制造材料;一种用数字光处理(DLP)打印的光聚合物树脂托盘材料和三种熔融沉积成型(FDM)打印的聚乳酸(PLA)、回收聚乳酸和聚对苯二甲酸乙二醇酯(PETG),以及一种传统的光固化丙烯酸树脂(LC PMMA)作为对照,来制作哑铃形(拉伸测试)、矩形(弯曲测试)试件,以验证其是否适合用于定制托盘(每组n = 10)。为了评估粘结强度,试件在0°、45°和90°的打印方向制作(每组n = 10)。用共聚焦扫描显微镜评估表面粗糙度。根据ISO 527 - 2和ISO 20795 - 1在万能材料试验机(英斯特朗)上完成三项机械测试。结果使用PRISM(版本10)软件进行统计分析,采用单因素方差分析和克鲁斯卡尔 - 沃利斯检验,设定统计学显著性为p < 0.05。进行共聚焦分析和扫描电子显微镜(SEM)分析以进行定量和定性的表面分析。

结果

对于拉伸强度和弯曲强度,PLA(回收)和PETG与LC PMMA相比无统计学显著差异(p > 0.05)。增材制造材料的粘结强度高于LC PMMA材料。发现打印方向会影响一些材料的粘结强度,表面粗糙度不同是影响因素之一。

结论

LC PMMA、PLA(回收)和PETG具有最大的弯曲强度和拉伸强度。就定制托盘的弯曲强度和拉伸强度而言,PLA(回收)和PETG是性能最佳的增材制造材料选项。与LC PMMA相比,所有增材制造材料的粘结强度均显著更高。为使粘结强度最大化,PLA(回收)应以0°角打印,PETG应以0°或90°角打印。牙科从业者除了要考虑材料的机械性能外,还应考虑材料不同程度的可回收性。

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