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溶剂萃取后用原子吸收分光光度法测定茶叶中微克量的铜。

Atomic absorption spectrophotometric determination of microgram quantities of copper in tea after solvent extraction.

作者信息

Aziz-Alrahman A M

出版信息

Int J Environ Anal Chem. 1985;22(3-4):251-7. doi: 10.1080/03067318508076424.

DOI:10.1080/03067318508076424
PMID:4077371
Abstract

An atomic absorption spectrophotometric method is described for determining trace amounts of copper in tea. The method is based on the solvent extraction of the metal as tetraiodocuprate (I), from 2 M HCl solutions of tea samples which contain 12% (w/v) KI, into methylisobutyl ketone. The organic extracts, containing the ion-association complex of copper are atomized into an air-acetylene flame. The limit of detection is 1.14 micrograms g-1 Cu.

摘要

描述了一种用于测定茶叶中痕量铜的原子吸收分光光度法。该方法基于将金属以四碘合铜(I)的形式从含有12%(w/v)碘化钾的茶叶样品的2M盐酸溶液中溶剂萃取到甲基异丁基酮中。含有铜离子缔合络合物的有机萃取物被雾化到空气 - 乙炔火焰中。检测限为1.14微克 g-1铜。

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