Cao Yuxi, Zuo Guofeng, Peng Yang, Zhu Lin, Tong Shuai, Yin Shubiao, Sun Xinjun
Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China.
Central Iron and Steel Research Institute Group, Engineering Steel Institute, Beiing 100081, China.
Materials (Basel). 2025 Jul 24;18(15):3462. doi: 10.3390/ma18153462.
Deep-sea oil and gas pipelines undergo significant plastic strain during reel-lay installation. Additionally, the static strain aging phenomenon that occurs during service can further deteriorate the mechanical properties of the pipelines. This study investigates the plastic deformation mechanism of reel-lay pipeline steel by subjecting the test steel to 5% pre-strain followed by aging treatment at 250 °C for 1 h. The present study systematically correlates the evolution of mechanical properties with microstructural changes through microstructural characterization techniques such as EBSD, TEM, and XRD. The results demonstrate that after pre-straining, the yield strength of the experimental steel increases due to dislocation strengthening and residual stress generation, while its uniform elongation decreases. Although no significant changes in grain size are observed macroscopically, microstructural characterization reveals a substantial increase in dislocation density within the matrix, forming dislocation cells and walls. These substructures lead to a deterioration of the material's work hardening capacity. Following aging treatment, the tested steel exhibits further increased yield strength and reduced uniform elongation. After aging treatment, although the dislocation density in the matrix slightly decreases and dislocation tangles are somewhat reduced, the Cottrell atmosphere pinning effect leads to a further decline in work hardening capability, ultimately resulting in the deterioration of plasticity in reel-lay pipeline steel. The instantaneous hardening exponent curve shows that the work hardening phenomenon becomes more pronounced in the tested steel after strain aging as the tempering temperature increases.
深海油气管道在卷筒铺设安装过程中会经历显著的塑性应变。此外,服役期间发生的静态应变时效现象会进一步恶化管道的力学性能。本研究通过对试验钢进行5%的预应变,然后在250℃下时效处理1小时,研究卷筒铺设管道钢的塑性变形机制。本研究通过电子背散射衍射(EBSD)、透射电子显微镜(TEM)和X射线衍射(XRD)等微观结构表征技术,系统地将力学性能的演变与微观结构变化联系起来。结果表明,预应变后,试验钢的屈服强度由于位错强化和残余应力的产生而增加,而其均匀伸长率降低。虽然宏观上未观察到晶粒尺寸有明显变化,但微观结构表征显示基体中位错密度大幅增加,形成了位错胞和位错壁。这些亚结构导致材料加工硬化能力下降。时效处理后,试验钢的屈服强度进一步提高,均匀伸长率降低。时效处理后,虽然基体中的位错密度略有降低,位错缠结有所减少,但柯氏气团钉扎效应导致加工硬化能力进一步下降,最终导致卷筒铺设管道钢的塑性恶化。瞬时硬化指数曲线表明,随着回火温度的升高,试验钢在应变时效后的加工硬化现象变得更加明显。