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西瓜汁微滤:优化以最大化抗氧化化合物并影响矿物质含量。

Watermelon juice microfiltration: optimization to maximize antioxidant compounds and influence mineral content.

作者信息

Lovato Frederico, Kowaleski Jussara, da Silva Sabrine Zambiazi, Kottwitz Luciana Bill Mikito, Martin Clayton Antunes, Tiuman Tatiana Shioji, Zara Ricardo Fiori

机构信息

Federal Technological University of Paraná, Cristo Rei Street, 19 Toledo, Toledo, Parana Brazil.

Fundetec - Foundation for Scientific and Technological Development, BR 277, km 573, Cascavel, Parana Brazil.

出版信息

J Food Sci Technol. 2025 Oct;62(10):1895-1904. doi: 10.1007/s13197-025-06202-5. Epub 2025 Jan 27.

Abstract

Traditional methods for fruit juice preservation use high temperatures, which degrade beneficial compounds like vitamins and antioxidants. Membrane filtration provides a gentler alternative, preserving nutrients through mild operating temperatures. This study assessed the temperature and pressure influence on watermelon juice microfiltration, focusing on permeated flow, lycopene, sugars, phenolic compounds, and flavonoids. Using a 2 composite design with central values, optimal conditions were determined by the desirability function, with pressure at 1.0 bar and temperature at 37ºC, maximizing these response variables. Resistance to permeated flux was primarily due to fouling, with an initial 25% flux reduction. The process effectively concentrated lycopene, sugars, phenolic compounds, and flavonoids, although mineral content decreased in both concentrated and permeated juice, with potassium being the most abundant mineral. The concentrated juice showed greater mineral loss than pasteurized due to retention during microfiltration. Under optimized conditions, microbial load reduction allowed the concentrated juice a shelf life comparable to pasteurized juice (14 days). Sensory analysis showed strong consumer acceptance, with 64% of tasters expressing purchase intent. These results suggest commercial viability for the concentrated juice; moreover, its high carotenoid retention could serve as an industrial ingredient for functional foods.

摘要

传统的果汁保鲜方法采用高温,这会使维生素和抗氧化剂等有益化合物降解。膜过滤提供了一种更温和的替代方法,通过温和的操作温度来保留营养成分。本研究评估了温度和压力对西瓜汁微滤的影响,重点关注渗透流量、番茄红素、糖分、酚类化合物和黄酮类化合物。采用具有中心值的二水平复合设计,通过合意性函数确定最佳条件,压力为1.0巴,温度为37ºC,使这些响应变量最大化。对渗透通量的阻力主要是由于污染,初始通量降低了25%。该过程有效地浓缩了番茄红素、糖分、酚类化合物和黄酮类化合物,尽管浓缩汁和渗透汁中的矿物质含量均有所下降,钾是含量最丰富的矿物质。由于在微滤过程中的截留,浓缩汁的矿物质损失比巴氏杀菌汁更大。在优化条件下,微生物负荷的降低使浓缩汁的保质期与巴氏杀菌汁相当(14天)。感官分析表明消费者接受度很高,64%的品尝者表示有购买意愿。这些结果表明浓缩汁具有商业可行性;此外,其高类胡萝卜素保留率可作为功能性食品的工业原料。

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