胶原蛋白交联的化学性质。几种胶原蛋白交联物和交联前体还原产物的简便合成方法。
The chemistry of the collagen cross-links. A convenient synthesis of the reduction products of several collagen cross-links and cross-link precursors.
作者信息
Davis N R, Bailey A J
出版信息
Biochem J. 1972 Aug;129(1):91-6. doi: 10.1042/bj1290091.
Abstract
New synthetic routes to the reduction products of several collagen cross-links and cross-link precursors are described. By the use of these routes hydroxynorleucine, 5,6-dihydroxynorleucine, hydroxylysinonorleucine and hydroxylysinohydroxynorleucine can be synthesized via one common synthetic intermediate. The synthetic routes provide a convenient source of these unusual amino acids, as well as confirming the structure of hydroxylysinohydroxynorleucine and the other lysine-derived residues found in borohydride-reduced collagens.
摘要
本文描述了几种胶原蛋白交联产物和交联前体还原产物的新合成路线。通过这些路线，羟基正亮氨酸、5,6-二羟基正亮氨酸、羟赖氨酰正亮氨酸和羟赖氨酰羟正亮氨酸可以通过一个共同的合成中间体进行合成。这些合成路线为这些特殊氨基酸提供了便利的来源，同时也证实了羟赖氨酰羟正亮氨酸以及在硼氢化钠还原的胶原蛋白中发现的其他赖氨酸衍生残基的结构。
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本文引用的文献
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Studies on the amide and C-terminal residues in proteins. 2. The ammonia nitrogen and amide nitrogen of various native protein preparations.蛋白质中酰胺和C末端残基的研究。2. 各种天然蛋白质制剂中的氨氮和酰胺氮。
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Biochemistry of collagen crosslinking. Isolation of a new crosslink, hydroxylysinohydroxynorleucine, and its reduced precursor, dihydroxynorleucine, from bovine tendon.胶原蛋白交联的生物化学。从牛腱中分离出一种新的交联物——羟赖氨酰羟正亮氨酸及其还原前体二羟正亮氨酸。
Biochem Biophys Res Commun. 1970 Dec 24;41(6):1597-604. doi: 10.1016/0006-291x(70)90571-1.
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In vitro studies on the enzymic biosynthesis of the collagen crosslinks.关于胶原蛋白交联酶促生物合成的体外研究。
Biochem Biophys Res Commun. 1970 Oct 9;41(1):251-9. doi: 10.1016/0006-291x(70)90496-1.
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Chemistry of the collagen cross-links. Isolation and characterization of two intermediate intermolecular cross-links in collagen.胶原蛋白交联的化学性质。胶原蛋白中两种中间分子间交联的分离与表征。
Biochem J. 1970 May;117(5):819-31. doi: 10.1042/bj1170819.
6
Isolation of lysinonorleucine from collagen.从胶原蛋白中分离赖氨酰正亮氨酸。
Biochem Biophys Res Commun. 1970 Apr 8;39(1):183-9. doi: 10.1016/0006-291x(70)90775-8.
7
The chemistry of the collagen cross-links. The absence of reduction of dehydrolysinonorleucine and dehydrohydroxylysinonorleucine in vivo.胶原蛋白交联的化学性质。体内脱氢赖氨酸正亮氨酸和脱氢羟赖氨酸正亮氨酸未发生还原反应。
Biochem J. 1971 Jan;121(2):257-9. doi: 10.1042/bj1210257.
8
Identification of two interchain crosslinks of bone and dentine collagen.骨和牙本质胶原蛋白两种链间交联的鉴定。
Biochem Biophys Res Commun. 1969 Jun 6;35(5):663-71. doi: 10.1016/0006-291x(69)90456-2.
9
Chemical synthesis of the reduced form of an intermolecular crosslink of collagen: a re-evaluation of the structure of syndesine.胶原蛋白分子间交联还原形式的化学合成：对羟赖氨酰吡啶交联结构的重新评估。
Biochem Biophys Res Commun. 1971 Dec 17;45(6):1416-22. doi: 10.1016/0006-291x(71)90178-1.
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