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[采用比色法和液相色谱法测定空气中的联苯胺]

[Determination of benzidine in the air using the colorimetry and liquid chromatography methods].

作者信息

Krajewski J, Ciosek A, Lipski K

出版信息

Med Pr. 1979;30(5):317-22.

PMID:514067
Abstract

The paper presents selection of analytical methods for determination of airborne benzidine, whose maximum admissible concentration (MAC) comes to zero. Colorimetric method with T chloroamine, allowing to determine 3 microgram of benzidine in m3 of the air, was evaluated. Such advantages of the method as specificity and availability of reagents and measuring apparatus were stressed. Another method presented in the paper is based on liquid chromatography, and its main features are: much better determinability of--0.7 microgram benzidine in m3 of the air and better precision than that of the colorimetric method. Its usefulness is however limited due to the necessity to have a very expensive liquid chromatograph.

摘要

本文介绍了空气中联苯胺测定分析方法的选择,其最大允许浓度(MAC)为零。对采用T氯胺的比色法进行了评估,该方法可测定空气中每立方米3微克的联苯胺。强调了该方法具有试剂和测量仪器特异性强且易于获得等优点。本文介绍的另一种方法基于液相色谱,其主要特点是:能更好地测定空气中每立方米0.7微克的联苯胺,且精密度比色法更好。然而,由于需要非常昂贵的液相色谱仪,其应用受到限制。

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