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Identification and characterization of the glucuronide metabolite of diethyldithiocarbamic acid in the bile from the isolated perfused rat liver by gas chromatography and mass spectrometry.

作者信息

Eneanya D I, Andresen B D, Gerber N, Bianchine J R

出版信息

Res Commun Chem Pathol Pharmacol. 1983 Sep;41(3):441-54.

PMID:6314458
Abstract

The glucuronide metabolite of diethyldithiocarbamic acid has been identified in bile from the isolated perfused rat liver. The bile was chromatographed on XAD-2 resin, pertrimethylsilylated with BSTAF + 1% TMCS, identified and characterized by combined gas chromatography and mass spectrometry. The glucuronide characterized as the silylated derivative showed no molecular ion but a small fragment ion at M-15(598).

摘要

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