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一种用于空气中硫化氢采样的新型被动式比色空气监测徽章的实验室验证和现场核查

Laboratory validation and field verification of a new passive colorimetric air monitoring badge for sampling hydrogen sulfide in air.

作者信息

Kring E V, Damrell D J, Henry T J, DeMoor H M, Basilio A N, Simon C E

出版信息

Am Ind Hyg Assoc J. 1984 Jan;45(1):1-9. doi: 10.1080/15298668491399271.

DOI:10.1080/15298668491399271
PMID:6702591
Abstract

The Pro-Tek passive colorimetric air monitoring badge for personal or area sampling of hydrogen sulfide is described. The badge has been validated over the range of 1.8 to 164 ppm-hours (0.23-21 ppm on an 8-hour TWA basis). It has an overall accuracy throughout this range of +/- 15.9% and meets the NIOSH accuracy criteria for an analytical and sampling method. The colorimetric analytical method used is based on the Texas Air Control Board's Molybdenum Blue method. Color-activated exposed badge solutions are read out on a standard laboratory spectrophotometer using 1 centimeter (10 mm) cells. Variations in exposure temperature (between 10 degrees and 40 degrees C), relative humidity, and face velocity (between 2 and 250 ft/min) do not affect badge performance. Unexposed badges are stable for more than 12 months refrigerated and for two months at room temperature.

摘要

介绍了用于个人或区域硫化氢采样的Pro-Tek被动比色空气监测徽章。该徽章在1.8至164 ppm-小时的范围内(基于8小时时间加权平均值为0.23-21 ppm)经过验证。在此范围内,其总体准确度为+/- 15.9%,符合美国国家职业安全与健康研究所(NIOSH)对分析和采样方法的准确度标准。所使用的比色分析方法基于得克萨斯州空气控制委员会的钼蓝法。使用1厘米(10毫米)比色皿,在标准实验室分光光度计上读取颜色激活的暴露徽章溶液。暴露温度(10摄氏度至40摄氏度之间)、相对湿度和表面风速(2至250英尺/分钟之间)的变化不会影响徽章性能。未暴露的徽章在冷藏条件下可稳定保存超过12个月,在室温下可稳定保存两个月。

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