Kusy R P, Leinfelder K F
J Biomed Mater Res. 1981 Mar;15(2):117-35. doi: 10.1002/jbm.820150202.
The age-hardening and tensile properties were determined for seven 10-14 kt. gold alloys, a conventional type II, and a sterling silver alloy. For the low-gold alloys the heat hardening curves indicated that the maximum aging effects were attained after 30 min at 400 degrees C. From tensile tests on either wire or dumbbell specimen configurations, Young's modulus (E), proportional limit (P.L.), ultimate tensile strength (U.T.S.), and elongation to break were measured for alloys in both the solution annealed (S) and the hardened (H) state. These stress-strain data not only confirmed previous correlations noted for conventional gold alloys between either E, P.L., or U.T.S. and hardness and between U.T.S. and P.L., but also varied systematically with the Au/Cu ratios in the (H) state. Under identical heat treatment and tensile testing conditions, comparison of the manufacturers' cast samples with this laboratory's specimens showed that, while the E, P.L., and U.T.S. differed somewhat, the greatest change occurred in the elongation to break. Here after measuring the porosity of the different specimen configurations and analyzing the log10 elongation with VHN, the conclusion was clear: Specimen geometry markedly influenced the physical properties. On this basis the proposed dumbbell geometry is advocated over the wire specimen configuration currently cited in ADA Specification No. 5.
对七种10 - 14克拉的金合金、一种传统的II型合金以及一种标准银合金测定了时效硬化和拉伸性能。对于低金合金,热硬化曲线表明在400℃下30分钟后达到最大时效效果。通过对丝状或哑铃状试样构型进行拉伸试验,测定了固溶退火(S)和硬化(H)状态下合金的杨氏模量(E)、比例极限(P.L.)、极限抗拉强度(U.T.S.)以及断裂伸长率。这些应力 - 应变数据不仅证实了先前关于传统金合金中E、P.L.或U.T.S.与硬度之间以及U.T.S.与P.L.之间的相关性,而且在硬化(H)状态下随金/铜比例有系统地变化。在相同的热处理和拉伸试验条件下,将制造商的铸造样品与本实验室的试样进行比较表明,虽然E、P.L.和U.T.S.略有不同,但断裂伸长率变化最大。在测量了不同试样构型的孔隙率并分析了维氏硬度(VHN)与对数断裂伸长率之后,结论很明确:试样几何形状显著影响物理性能。在此基础上,建议采用哑铃状几何形状,而不是ADA规范第5号中目前引用的丝状试样构型。