Delbeke F T, Debackere M, Jonckheere J A, De Leenheer A P
J Chromatogr. 1983 Mar 11;273(1):141-9.
A sensitive and rapid method for the gas chromatographic (with electron-capture detection) confirmation of derivable sympathomimetic amines is described. Extractive derivatization with pentafluorobenzoyl chloride is performed on 2-ml urine or plasma samples. Especially for primary amines, the method appears to be very sensitive. Mass spectral data allowed confirmation of the monobenzoylation of all congeners.
描述了一种用于气相色谱（带电子捕获检测）确证可衍生拟交感神经胺的灵敏且快速的方法。用五氟苯甲酰氯进行萃取衍生化反应，对2毫升尿液或血浆样本进行操作。特别是对于伯胺，该方法似乎非常灵敏。质谱数据可确证所有同系物的单苯甲酰化。
