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[新型色谱法。天然产物的分离与提纯技术]

[New chromatography. Technics for the isolation and separation of natural products].

作者信息

Hostettmann K

出版信息

Naturwissenschaften. 1983 Apr;70(4):186-9. doi: 10.1007/BF01047556.

DOI:10.1007/BF01047556
PMID:6855922
Abstract

Besides high-performance liquid chromatography (HPLC) which is now a well-established and currently used technique, several emerging methods for the isolation and separation of natural products are receiving considerable attention. Centrifugal thin-layer chromatography is a very rapid technique, but limited in resolution. Of special interest are the recently developed support-free liquid-liquid chromatography methods such as droplet counter-current chromatography (DCCC) and rotation locular counter-current chromatography (RLCC). This latter method was applied to the separation of the enantiomers of (+/-)-norephedrine.

摘要

除了高效液相色谱法（HPLC）这一现已成熟且仍在使用的技术外，几种新兴的天然产物分离和提纯方法也备受关注。离心薄层色谱法是一种非常快速的技术，但分辨率有限。特别值得关注的是最近开发的无载体液-液色谱法，如液滴逆流色谱法（DCCC）和旋转腔逆流色谱法（RLCC）。后一种方法被应用于（±）-去甲麻黄碱对映体的分离。

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本文引用的文献

1
Inhibition of type A and type B monoamine oxidase by isogentisin and its 3-O-glucoside.异荭草苷及其3-O-葡萄糖苷对A型和B型单胺氧化酶的抑制作用。
Planta Med. 1980 May;39(1):19-23. doi: 10.1055/s-2008-1074899.
2
Droplet countercurrent chromatography.
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3
Countercurrent chromatography with a new horizontal flow-through coil planet centrifuge.采用新型水平流通盘管式行星离心机的逆流色谱法。
Anal Biochem. 1979 Dec;100(2):271-81. doi: 10.1016/0003-2697(79)90230-6.