用石墨炉原子吸收分光光度法测定生物体液中的铝（作者译）

[Estimation of aluminium in biological fluids by atomic absorption spectrophotometry in a graphite oven (author's transl)].

作者信息

Clavel J P, Jaudon M C, Galli A

出版信息

Ann Biol Clin (Paris). 1978;36(1):33-8.

Abstract

The possibilities of use of a graphite oven type HGA 74 (Perkin Elmer) for the estimation of aluminium in biological fluids by atomic absorption spectrophotometry are described, with a special study of the stages of drying, mineralisation, atomisation, flow of inert gas, requirement for correction of non-specific absorption, etc. Under fixed experimental conditions, the limit of sensitivity (absorption 1%) was 2.28.10.(-11) grams and the linearity was good up to 100 microgram/l. This method of analysis by direct treatment of the samples required only small volumes of the latter and reduces the risk of contamination.

摘要

描述了使用石墨炉HGA 74型（珀金埃尔默公司）通过原子吸收分光光度法测定生物流体中铝的可能性，并特别研究了干燥、矿化、原子化、惰性气体流量、非特异性吸收校正要求等阶段。在固定的实验条件下，灵敏度极限（吸光度1%）为2.28×10⁻¹¹克，线性在高达100微克/升时良好。这种直接处理样品的分析方法仅需要少量样品，并降低了污染风险。