Johnson K E, Treble R G
Department of Chemistry, University of Regina, Saskatchewan, Canada.
J Clin Lab Anal. 1992;6(5):264-8. doi: 10.1002/jcla.1860060504.
Detailed procedures were developed for the furnace atomic absorption spectrophotometry (FAAS) determination of aluminum (Al) in serum, urine, cerebrospinal fluid (CSF), and proportionated dialysate. Of particular note were the use of Mg (NO3)2.6H2O as a matrix modifier and the employment of the standard additions routine in analysis. The accuracy of the method(s) used is supported by work with assayed controls and by recovery studies. The use of a "clean room" was shown to be unnecessary. Normal serum, urine, and CSF Al ranges observed were 4.8-8.9, 5.1-9.1, and 1.0-5.8 micrograms L-1 respectively.
已制定了详细程序,用于通过火焰原子吸收分光光度法(FAAS)测定血清、尿液、脑脊液(CSF)和比例透析液中的铝(Al)。特别值得注意的是,使用Mg(NO3)2·6H2O作为基体改进剂,并在分析中采用标准加入法。使用经过分析的对照品以及回收率研究证实了所采用方法的准确性。结果表明无需使用“洁净室”。观察到的正常血清、尿液和脑脊液中铝的范围分别为4.8 - 8.9、5.1 - 9.1和1.0 - 5.8微克/升。