博来霉素的化学。十八。碳-13核磁共振研究。
Chemistry of bleomycin. XVIII. carbon-13 NMR studies.
作者信息
Naganawa H, Muraoka Y, Takita T, Umezawa H
出版信息
J Antibiot (Tokyo). 1977 May;30(5):388-96. doi: 10.7164/antibiotics.30.388.
PMID:69623
Abstract
During chemical studies of bleomycin, many fragments and derivatives have been isolated and characterized. The 13C-NMR spectra of these compounds were taken and analyzed for structural information, and the complete assignment of the spectra was achieved. The 13C-chemical shift map thus obtained contains information about the structure and conformation and will be useful for studies on the chemistry and biology of bleomycin and related compounds.
摘要
在对博来霉素进行化学研究的过程中，已分离并表征了许多片段和衍生物。测定了这些化合物的13C-NMR光谱，并对其进行分析以获取结构信息，从而完成了光谱的完全归属。由此获得的13C化学位移图谱包含有关结构和构象的信息，将有助于博来霉素及相关化合物的化学和生物学研究。
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