Akhtar M H
J Chromatogr. 1982 Sep 3;246(1):81-7. doi: 10.1016/s0021-9673(00)82784-3.
A gas chromatographic method is described for the detection and estimation of deltamethrin in spiked samples of urine, feces, milk, liver, kidney, muscle and subcutaneous fat. It involved extraction with acetone, with the exception of milk and urine samples, liquid-liquid partition with acetonitrile, followed by clean-up on a micro-column using benzene-hexane (1:1) solvent system. Milk and urine samples were extracted with hexane followed by liquid-liquid partition with acetonitrile. Under the gas chromatographic conditions employed, deltamethrin eluted in less than 4 min.
描述了一种气相色谱法，用于检测和估算加标尿样、粪便、牛奶、肝脏、肾脏、肌肉和皮下脂肪中的溴氰菊酯。除牛奶和尿样外，用丙酮进行萃取，用乙腈进行液 - 液分配，然后使用苯 - 己烷（1:1）溶剂系统在微柱上进行净化。牛奶和尿样先用己烷萃取，然后用乙腈进行液 - 液分配。在所采用的气相色谱条件下，溴氰菊酯在不到4分钟内洗脱出来。
