Baker P B, Gough T A
J Chromatogr Sci. 1981 Oct;19(10):483-9. doi: 10.1093/chromsci/19.10.483.
The separation of heroin from other narcotic components of illicit preparations is achieved by high performance liquid chromatography. Using an aminopropyl bonded silica packing and a mixture of 85% acetonitrile and 15% 0.005 M tetrabutylammonium phosphate as the mobile phase, caffeine, heroin, acetylcodeine, 6-acetylmorphine, codeine, and morphine are separated from each other and are accurately quantified. Papaverine, noscapine, thebaine, and strychnine are also separated from these principal components.
通过高效液相色谱法可将海洛因与非法制剂中的其他麻醉成分分离。使用氨丙基键合硅胶填料，并以85%乙腈和15% 0.005 M磷酸四丁铵的混合物作为流动相，可将咖啡因、海洛因、乙酰可待因、6-乙酰吗啡、可待因和吗啡彼此分离并进行准确定量。罂粟碱、那可汀、蒂巴因和士的宁也可与这些主要成分分离。
