Hollifield H C, Breder C V, Dennison J L, Roach J A, Adams W S
J Assoc Off Anal Chem. 1980 Mar;63(2):173-7.
Samples of maple sirup and associated plastic packaging were examined for the presence of methyl methacrylate, toluene, and styrene by a head space gas chromatographic procedure. The volatile components common to the sirup and the plastic container were identified by gas chromatography-mass spectrometry. The quantities of these contaminants in the sirup were determined at ppb levels by the standard additions technique and repetitive headspace analysis.
采用顶空气相色谱法对枫糖浆样品及其相关塑料包装进行了甲基丙烯酸甲酯、甲苯和苯乙烯含量的检测。通过气相色谱-质谱联用仪鉴定了糖浆和塑料容器中常见的挥发性成分。采用标准加入法和重复顶空分析法测定了糖浆中这些污染物的含量,检测限为十亿分之一(ppb)水平。