Turnes M I, Rodriguez I, Mejuto M C, Cela R
Departamento de Química Analítica, Nutrición y Bromatología, Universidad de Santiago de Compostela, Spain.
J Chromatogr A. 1994 Oct 14;683(1):21-9. doi: 10.1016/S0021-9673(94)89098-6.
The use of an atomic emission detector following a process of preconcentration of drinking water samples by a factor of 1500:1 allows the highly selective determination of chlorophenols present in samples below the maximum limit of 0.5 ng/ml set by international regulations. The preconcentration of the samples is carried out using 0.25-g commercial graphitized carbon cartridges without the need for sample derivatization prior to solid-phase extraction.
在将饮用水样品预浓缩1500倍后使用原子发射检测器,能够高度选择性地测定样品中低于国际法规设定的0.5 ng/ml最大限量的氯酚。样品的预浓缩使用0.25克商用石墨化碳柱进行,在固相萃取之前无需对样品进行衍生化处理。