Iablochkin V D
Sud Med Ekspert. 1993 Jan-Mar;36(1):36-8.
The conditions of direct gas chromatographic assessment of barbiturates in reference solutions and cadaveric material extracts were analyzed with the aim of their unification. Along with the Kovach indexes, their temperature coefficients seem promising for the identification of barbiturates. Critical parameters of the evaporator temperature regimen were established, that may be used for barbiturate identification as well. The threshold values of gas chromatographic detection of phenobarbital, barbital, etaminal, hexenal, quietal, and hexobarbital were determined.
为实现巴比妥类药物分析条件的统一，对其在对照溶液和尸体材料提取物中的直接气相色谱评估条件进行了分析。除 Kovach 指数外，其温度系数在巴比妥类药物鉴定方面似乎也很有前景。确定了蒸发器温度控制的关键参数，该参数也可用于巴比妥类药物的鉴定。测定了苯巴比妥、巴比妥、戊巴比妥、己烯巴比妥、司可巴比妥和己巴比妥的气相色谱检测阈值。
