Henle T, Walter A W, Klostermeyer H
Lehrstuhl für Milchwissenschaft, Technische Universität München, Freising-Weihenstephan, Germany.
Z Lebensm Unters Forsch. 1994 Jan;198(1):66-7. doi: 10.1007/BF01195287.
After heating N alpha-acetyllysine and glucose for 4 h at 90 degrees C in the dry state and subsequent acid hydrolysis with 7.8 N HCl, preparative fractionation of the dihydrochlorides of furosine and pyridosine was achieved by cation-exchange chromatography. The lysine derivatives could be prepared with high yield and sufficient purity for the use as reference material.
将Nα-乙酰赖氨酸和葡萄糖在干燥状态下于90℃加热4小时，随后用7.8N盐酸进行酸水解，通过阳离子交换色谱法对呋喃素和吡啶素的二盐酸盐进行制备性分离。可以高收率和足够的纯度制备赖氨酸衍生物，用作参考物质。
