Hormazabal V, Steffenak I, Yndestad M
Department of Food Hygiene, Norwegian College of Veterinary Medicine, Oslo.
J Chromatogr. 1993 Jun 23;616(1):161-5. doi: 10.1016/0378-4347(93)80484-l.
A simple and rapid high-performance liquid chromatographic method for the simultaneous extraction and determination of residues of florfenicol and its metabolite florfenicol amine in fish tissue, muscle and liver has been developed. The calibration curves were linear, the recovery of florfenicol was 99-107%, and the recovery of florfenicol amine was 94-100%. The detection limits for florfenicol and florfenicol amine were 20 ng/g in muscle and 50 ng/g in liver.
已开发出一种简单快速的高效液相色谱法，用于同时提取和测定鱼组织、肌肉和肝脏中氟苯尼考及其代谢物氟苯尼考胺的残留量。校准曲线呈线性，氟苯尼考的回收率为99 - 107%，氟苯尼考胺的回收率为94 - 100%。氟苯尼考和氟苯尼考胺在肌肉中的检测限为20 ng/g，在肝脏中的检测限为50 ng/g。
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