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用薄层色谱法分离和测定有机氯农药及其在毒理学分析中的应用。

Isolation and determination of chlorinated organic pesticides by thin-layer chromatography and the application to toxicological analysis.

作者信息

Tewari S N, Sharma I C

出版信息

J Chromatogr. 1977 Jan 21;131:275-84. doi: 10.1016/s0021-9673(00)80942-5.

DOI:10.1016/s0021-9673(00)80942-5
PMID:856854
Abstract

A sensitive method for the isolation and clean-up of chlorinated organic pesticides from tissues and biological materials is discussed. RF values of the pesticides in 26 solvent systems, and colours of the spots given with various chromogenic reagents, are reported. The limits of detection, and densitometric measurements, are also discussed. The average recovery has been found to be 94%. The distribution of endrin in different autopsy tissues from five different victims has been studied by the proposed technique.

摘要

本文讨论了一种从组织和生物材料中分离和净化有机氯农药的灵敏方法。报告了26种溶剂系统中农药的比移值,以及各种显色剂产生的斑点颜色。还讨论了检测限和光密度测量。已发现平均回收率为94%。利用所提出的技术研究了来自五名不同受害者的不同尸检组织中异狄氏剂的分布情况。

相似文献

1
Isolation and determination of chlorinated organic pesticides by thin-layer chromatography and the application to toxicological analysis.用薄层色谱法分离和测定有机氯农药及其在毒理学分析中的应用。
J Chromatogr. 1977 Jan 21;131:275-84. doi: 10.1016/s0021-9673(00)80942-5.
2
Detection and determination of organophosphorus insecticides in tissues by thin-layer chromatography.
J Chromatogr. 1977 Jan 11;130:229-36. doi: 10.1016/s0021-9673(00)89799-x.
3
Detection and quantitative determination of certain chlorinated pesticides by micro-thin layer chromatography.用微量薄层色谱法检测和定量测定某些氯化农药。
J Chromatogr. 1971 Nov 26;62(3):479-84. doi: 10.1016/s0021-9673(00)91404-3.
4
[Beta-rodamine as a chromogenic agent in thin layer chromatography of chlorinated insecticides].
Rev Farm Bioquim Univ Sao Paulo. 1971 Jan-Jun;9(1):223-34.
5
Thin-layer and gas chromatography techniques for the isolation and identification of carbamate pesticides in post mortem material.用于死后材料中氨基甲酸酯类农药分离与鉴定的薄层色谱法和气相色谱法技术
Acta Med Leg Soc (Liege). 1985;35(1):190-8.
6
[Method of extraction and purification of chlorinated pesticides from biological material for toxicological purposes].
Arq Inst Biol (Sao Paulo). 1971 Jul-Sep;38(3):115-23.
7
[Pesticide residues on tobacco products. 1. Chlorinated hydrocarbon content of our tobacco products].[烟草制品上的农药残留。1. 我们烟草制品中的氯代烃含量]
Nahrung. 1972;16(4):353-8.
8
Thin-layer chromatographic technique for the separation and identification of carbamate pesticides in post mortem material.用于死后材料中氨基甲酸酯类农药分离与鉴定的薄层色谱技术。
J Chromatogr. 1979 Apr 21;172:528-30. doi: 10.1016/s0021-9673(00)91013-6.
9
Determination of polychlorinated biphenyls in the presence of organochlorine pesticides by thin-layer chromatography.在有机氯农药存在的情况下,用薄层色谱法测定多氯联苯。
Environ Lett. 1973;4(3):201-10. doi: 10.1080/00139307309436597.
10
[The isolation and detection of actellic by thin-layer chromatography in the forensic chemical study of cadaveric organs].[在尸体器官法医化学研究中用薄层色谱法分离和检测速灭威]
Sud Med Ekspert. 1994 Jan-Mar;37(1):28-30.

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Levels of organochlorine pesticides in the blood of people living in areas of intensive pesticide use in Sudan.苏丹农药密集使用地区居民血液中有机氯农药的含量
Environ Monit Assess. 2015 Mar;187(3):68. doi: 10.1007/s10661-015-4269-0. Epub 2015 Feb 3.