Font G, Mañes J, Moltó J C, Picó Y
Laboratori de Bromatologia i Toxicologia, Facultat de Farmàcia, Universitat de Valéncia, Spain.
J Chromatogr A. 1996 May 10;733(1-2):449-71. doi: 10.1016/0021-9673(95)00972-8.
A review and discussion of the analytical developments of the last 10 years in the determination of polychlorinated biphenyls (PCBs) in water are presented, including sample treatment, clean-up, identification and determination. Some of the most significant advances have occurred in the area of sample preparation, such as the increased adoption of solid-phase extraction and on-line techniques and the chromatographic separation of PCB congeners, principally by mass spectrometry. Special attention is focused on applications to real samples.
本文综述并讨论了过去十年中水中多氯联苯（PCBs）测定方法的分析进展，包括样品处理、净化、鉴定和测定。一些最重要的进展出现在样品制备领域，例如固相萃取和在线技术的更多应用，以及主要通过质谱对多氯联苯同系物进行色谱分离。特别关注了在实际样品中的应用。
