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Determination of terbacil in soil by gas-liquid chromatography with 63Ni electron capture detection.

作者信息

Khan S U

出版信息

Bull Environ Contam Toxicol. 1977 Jul;18(1):83-8. doi: 10.1007/BF01686310.

DOI:10.1007/BF01686310
PMID:884341
Abstract

A method is described for the determination of terbacil residue in soil. The herbicide residue is extracted with 1.5% NaOH, partitioned into an organic phase and subsequently cleaned up by passing through a Florisil column. Extract is analyzed by gas-liquid chromatography using a 63Ni electron capture detector. The procedure has a sensitivity of about 0.01 ppm, based on a 20 g sample. The method was used for the analysis of terbacil residues in the field treated soil samples.

摘要

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本文引用的文献

1
Synthesis and studies with labeled bromacil 2-C14 and terbacil.
J Agric Food Chem. 1969 Sep;17(5):980-6. doi: 10.1021/jf60165a031.