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司法样本中苯乙胺的鉴定。

Identification of alpha-phenylethylamine in judicial samples.

作者信息

Meyer E, Van Bocxlaer J F, Lambert W E, Thienpont L, De Leenheer A P

机构信息

Laboratorium voor Toxicologie, Universiteit Gent, Belgium.

出版信息

J Anal Toxicol. 1996 Mar-Apr;20(2):116-20. doi: 10.1093/jat/20.2.116.

DOI:10.1093/jat/20.2.116
PMID:8868403
Abstract

alpha-Phenylethylamine was recently identified in samples from several judicial cases using chromatographic (high-performance liquid chromatography-diode-array detection, gas chromatography-mass spectrometry, and gas chromatography-Fourier transform infrared detection) and spectrometric (nuclear magnetic resonance) techniques. In the first case, 1 kg of a white powder was found in a basement laboratory. It contained caffeine and more than 15% alpha-phenylethylamine. In the second case, two white powders were seized from a female. One powder consisted of pure amphetamine, and the other was a mixture of caffeine, amphetamine, and alpha-phenylethylamine. Four months later, a couple, who were known drug users, were found dead in their apartment. Urine samples of both victims contained large amounts of amphetamine together with alpha-phenylethylamine. Recently, 0.13 kg of a white powder and 0.30 kg of an orange powder were seized during a law enforcement operation. Both powders were mixtures of caffeine, amphetamine, and alpha-phenylethylamine. The data presented demonstrate the recent and unrelated repetitive occurrence of alpha-phenylethylamine in the circuit of illicit drugs.

摘要

最近,通过色谱法(高效液相色谱 - 二极管阵列检测、气相色谱 - 质谱联用以及气相色谱 - 傅里叶变换红外检测)和光谱法(核磁共振)技术,在几起司法案件的样本中发现了α - 苯乙胺。在第一起案件中,在一个地下室实验室发现了1千克白色粉末。其中含有咖啡因以及超过15%的α - 苯乙胺。在第二起案件中,从一名女性身上查获了两种白色粉末。一种粉末是纯苯丙胺,另一种是咖啡因、苯丙胺和α - 苯乙胺的混合物。四个月后,一对已知的吸毒夫妇被发现死于他们的公寓。两名受害者的尿液样本中都含有大量的苯丙胺以及α - 苯乙胺。最近,在一次执法行动中查获了0.13千克白色粉末和0.30千克橙色粉末。两种粉末都是咖啡因、苯丙胺和α - 苯乙胺的混合物。所呈现的数据表明,α - 苯乙胺最近在非法药物流通中反复出现且互不相关。

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