Rose H
Ultramicroscopy. 1977 Apr;2(2-3):251-67. doi: 10.1016/s0304-3991(76)91538-2.
A rigorous treatment of image formation, taking into account inelastic scattering and partially coherent illumination, is given for the CTEM. The results also hold for a STEM if the momentum vectors of the incident and outgoing waves are interchanged and the flight direction of the electrons is reversed. A generalized optical theorem is found which connects the anti-Friedel part of the elastic scattering amplitude with the squares of the elastic and inelastic scattering amplitudes. This theorem has important consequences for all approximation methods. For example, it shows that inelastic scattering influences the elastic scattering amplitude. It is further shown that the observed wings in optical diffractograms, obtained from micrographs of amorphous material taken using tilted beam illumination, can only be explained if double scattering (elastic and inelastic) is assumed. Hollow-cone illumination strongly suppresses the structural noise in the phase contrast image. The corresponding phase contrast transfer function (PCTF) is calculated for two different cone angles, assuming that no beam-limiting aperture is present. In addition, the PCTFs of a corrected microscope are calculated for two different illumination modes, one yielding negative and the other positive phase contrast. Finally, the contrast transfer has been investigated for a stem operating with a split detector.
针对透射电子显微镜(CTEM),给出了一种考虑非弹性散射和部分相干照明的严格图像形成处理方法。如果将入射波和出射波的动量矢量互换,并反转电子的飞行方向,该结果对于扫描透射电子显微镜(STEM)同样成立。发现了一个广义光学定理,它将弹性散射振幅的反弗里德尔部分与弹性和非弹性散射振幅的平方联系起来。该定理对所有近似方法都有重要影响。例如,它表明非弹性散射会影响弹性散射振幅。进一步表明,从使用倾斜束照明拍摄的非晶材料显微照片获得的光学衍射图中观察到的翼状图案,只有在假设存在双散射(弹性和非弹性)的情况下才能得到解释。空心锥照明强烈抑制相衬图像中的结构噪声。在假设不存在束限制孔径的情况下,针对两种不同的锥角计算了相应的相衬传递函数(PCTF)。此外,针对两种不同的照明模式计算了校正显微镜的PCTF,一种产生负相衬,另一种产生正相衬。最后,研究了使用分离探测器运行的扫描透射电子显微镜的对比度传递。