Miyazaki M, Sato M, Onose H, Moore B K
Nihon University School of Dentistry, Dept. of Operative Dentistry, Chiyoda-ku, Tokyo, Japan.
Am J Dent. 1998 Jun;11(3):118-22.
To investigate the influence of thermal cycling on bond strength to dentin of 2-step bonding systems.
The systems used were self-etching primer systems; Fluoro Bond (FB), Liner Bond II (LB), and Mac Bond II (MB); and self-priming adhesive systems; One-Step (OS), OptiBond Solo (OB), Prime & Bond 2.0 (PB), and Single Bond (SB). Bovine mandibular incisors were mounted in self-curing resin and the facial surfaces were wet ground with #600 SiC paper. Enamel and dentin surfaces were treated following each manufacturers' instructions. Adhesives were applied and composites were condensed into a Teflon mold (4x2 mm) placed on the dentin surface and light activated. Bonded specimens were divided into four groups; (a) stored in 37 degrees C water for 24 hours, (b) stored in 37 degrees C water for 24 hours followed by subjecting to thermal cycling between 5 degrees C and 60 degrees C for 3,000 times, (c) 10,000 times, and (d) 30,000 times. Twelve samples per test group were shear tested at a crosshead speed of 1.0 mm/minute. One-way ANOVAs followed by Duncan's multiple range test (P < 0.05) were performed.
For FB, LB, and MB, a small decrease in bond strength was observed and no significant differences were observed among the thermal cycling groups. For OS, OB, PB, and SB, a significant decrease in bond strength was observed for the 30,000 thermal cycling groups. The changes in bond strength after TC were different between the bonding systems.
研究热循环对两步法粘结系统与牙本质粘结强度的影响。
所用系统为自酸蚀底漆系统,即氟粘结剂(FB)、Ⅱ型衬层粘结剂(LB)和Ⅱ型强力粘结剂(MB);以及自粘结底漆系统,即一步法粘结剂(OS)、单组分光固化粘结剂(OB)、2.0型粘结剂(PB)和单键粘结剂(SB)。将牛下颌切牙固定于自凝树脂中,其唇面用600号碳化硅砂纸湿磨。按照各制造商的说明处理釉质和牙本质表面。涂抹粘结剂,将复合树脂填入置于牙本质表面的聚四氟乙烯模具(4×2毫米)中并光固化。将粘结标本分为四组:(a)在37℃水中储存24小时;(b)在37℃水中储存24小时,然后在5℃至60℃之间进行3000次热循环;(c)10000次;(d)30000次。每个测试组的12个样本以1.0毫米/分钟的十字头速度进行剪切测试。进行单因素方差分析,随后进行邓肯多重极差检验(P<0.05)。
对于FB、LB和MB,观察到粘结强度略有下降,热循环组之间未观察到显著差异。对于OS、OB、PB和SB,30000次热循环组的粘结强度显著下降。热循环后粘结强度的变化在不同粘结系统之间有所不同。