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热循环对两步法粘结系统牙本质粘结强度的影响。

Influence of thermal cycling on dentin bond strength of two-step bonding systems.

作者信息

Miyazaki M, Sato M, Onose H, Moore B K

机构信息

Nihon University School of Dentistry, Dept. of Operative Dentistry, Chiyoda-ku, Tokyo, Japan.

出版信息

Am J Dent. 1998 Jun;11(3):118-22.

PMID:9823072
Abstract

PURPOSE

To investigate the influence of thermal cycling on bond strength to dentin of 2-step bonding systems.

MATERIALS AND METHODS

The systems used were self-etching primer systems; Fluoro Bond (FB), Liner Bond II (LB), and Mac Bond II (MB); and self-priming adhesive systems; One-Step (OS), OptiBond Solo (OB), Prime & Bond 2.0 (PB), and Single Bond (SB). Bovine mandibular incisors were mounted in self-curing resin and the facial surfaces were wet ground with #600 SiC paper. Enamel and dentin surfaces were treated following each manufacturers' instructions. Adhesives were applied and composites were condensed into a Teflon mold (4x2 mm) placed on the dentin surface and light activated. Bonded specimens were divided into four groups; (a) stored in 37 degrees C water for 24 hours, (b) stored in 37 degrees C water for 24 hours followed by subjecting to thermal cycling between 5 degrees C and 60 degrees C for 3,000 times, (c) 10,000 times, and (d) 30,000 times. Twelve samples per test group were shear tested at a crosshead speed of 1.0 mm/minute. One-way ANOVAs followed by Duncan's multiple range test (P < 0.05) were performed.

RESULTS

For FB, LB, and MB, a small decrease in bond strength was observed and no significant differences were observed among the thermal cycling groups. For OS, OB, PB, and SB, a significant decrease in bond strength was observed for the 30,000 thermal cycling groups. The changes in bond strength after TC were different between the bonding systems.

摘要

目的

研究热循环对两步法粘结系统与牙本质粘结强度的影响。

材料与方法

所用系统为自酸蚀底漆系统,即氟粘结剂(FB)、Ⅱ型衬层粘结剂(LB)和Ⅱ型强力粘结剂(MB);以及自粘结底漆系统,即一步法粘结剂(OS)、单组分光固化粘结剂(OB)、2.0型粘结剂(PB)和单键粘结剂(SB)。将牛下颌切牙固定于自凝树脂中,其唇面用600号碳化硅砂纸湿磨。按照各制造商的说明处理釉质和牙本质表面。涂抹粘结剂,将复合树脂填入置于牙本质表面的聚四氟乙烯模具(4×2毫米)中并光固化。将粘结标本分为四组:(a)在37℃水中储存24小时;(b)在37℃水中储存24小时,然后在5℃至60℃之间进行3000次热循环;(c)10000次;(d)30000次。每个测试组的12个样本以1.0毫米/分钟的十字头速度进行剪切测试。进行单因素方差分析,随后进行邓肯多重极差检验(P<0.05)。

结果

对于FB、LB和MB,观察到粘结强度略有下降,热循环组之间未观察到显著差异。对于OS、OB、PB和SB,30000次热循环组的粘结强度显著下降。热循环后粘结强度的变化在不同粘结系统之间有所不同。

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