Cecchi L, Volonterio G, Resmini P
S TA NU. 1976 Mar-Apr;6(2):119-21.
The influence on liquid scintillation counting efficiency of internal standards toluene-14C, hexadecane-14C and ethanol-14C has been studied for low level-14C measuring of ethanol samples. Many biological and synthetic samples of ethanol have been counted: the best results are obtained with external standardisation on quenching calibration curve made with ethanol-14C. External standardisation on quenching calibration curve made with toluene-14C is preferable to internal standardisation with ethanol-14C. Hesadecane-14C as internal standard gives activities rather higher than true values.
针对乙醇样品中低水平碳-14的测量,研究了内标物甲苯-14C、十六烷-14C和乙醇-14C对液体闪烁计数效率的影响。对许多乙醇的生物和合成样品进行了计数:使用乙醇-14C制作的猝灭校准曲线上进行外标法可获得最佳结果。用甲苯-14C制作的猝灭校准曲线上进行外标法比用乙醇-14C进行内标法更可取。十六烷-14C作为内标给出的活度比真实值高得多。