Keller T, Schneider A, Regenscheit P, Dirnhofer R, Rücker T, Jaspers J, Kisser W
Institute of Forensic Medicine, University of Salzburg, Austria.
Forensic Sci Int. 1999 Jan 11;99(2):93-105. doi: 10.1016/s0379-0738(98)00168-6.
A new method has been developed for the rapid analysis of psilocybin and/or psilocin in fungus material using ion mobility spectrometry. Quantitative analysis was performed by gas chromatography-mass spectrometry after a simple one-step extraction involving homogenization of the dried fruit bodies of fungi in chloroform and derivatization with MSTFA. The proposed methods resulted in rapid procedures useful in analyzing psychotropic fungi for psilocybin and psilocin.
已开发出一种新方法，用于使用离子迁移谱快速分析真菌材料中的裸盖菇素和/或脱磷酸裸盖菇素。通过气相色谱-质谱联用仪进行定量分析，该分析经过一个简单的一步萃取过程，即将真菌干燥子实体在氯仿中匀浆并用N-甲基-N-（三甲基硅烷基）三氟乙酰胺进行衍生化。所提出的方法产生了可用于分析致幻真菌中裸盖菇素和脱磷酸裸盖菇素的快速程序。
