Meisinger F, Steinbereithner K, Wliszczak W
Anaesthesist. 1976 Dec;25(12):588-91.
A simple procedure enabling defined (standard) gas concentrations of volatile anaesthetics to be prepared for gas chromatographic analyses in a short time is described. Results obtained with this technique, showing excellent reproducibility (coefficients of variation: 1 per cent or less), are presented. Sources of error inherent in the method theoretically (dilution effect of repeated sampling; not taking into account nonideality of gas mixtures) are discussed, these errors, as easily may be proven, being within the limits of accuracy of the analytical method.
本文描述了一种简单的方法,该方法能够在短时间内制备出用于气相色谱分析的特定(标准)浓度挥发性麻醉剂气体。文中给出了用该技术获得的结果,这些结果显示出极佳的重现性(变异系数:1%或更低)。从理论上讨论了该方法固有的误差来源(重复采样的稀释效应;未考虑气体混合物的非理想性),且易于证明这些误差在分析方法的准确度范围内。