Yun K, Wang Y, Li G, Wang Y
Department of Forensic Medicine, Shanxi Medical University, Taiyuan.
Fa Yi Xue Za Zhi. 1997;13(2):77-8, inside back cover.
A rapid qualitative and quantitative analysis of fluoroacetatamide and fluoroacetic acid in rodenticides by capillary gaschromatography was described in this paper. Isoamyl alcohol was used as the internal standard. The determination curves of fluoroacetatamide and fluoroacetic acid in rodenticides were linear in the ranges of 0.0625-4 mg/ml and 0.625-20 mg/ml. The detection limits of fluoroacetatamide and fluoroacetic acid were 31.25 micrograms/ml (32.5 ng) and 625 micrograms/ml (625 ng), 87.5% and 30% of rodenticides sold in Taiyuan ground market from May, 1995 to May, 1996 contain fluoroacetatamide and fluoroacetic acid.
本文描述了用毛细管气相色谱法对灭鼠剂中氟乙酰胺和氟乙酸进行快速定性和定量分析。以异戊醇为内标。灭鼠剂中氟乙酰胺和氟乙酸的测定曲线在0.0625 - 4毫克/毫升和0.625 - 20毫克/毫升范围内呈线性。氟乙酰胺和氟乙酸的检测限分别为31.25微克/毫升（32.5纳克）和625微克/毫升（625纳克），1995年5月至1996年5月在太原地面市场销售的灭鼠剂中，87.5%含有氟乙酰胺，30%含有氟乙酸。
