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用于正畸带环粘结的树脂改性玻璃离子水门汀的体外研究。隔离、多余材料去除及湿度作为影响釉质、水门汀与金属之间粘结强度的因素。

In-vitro study of resin-modified glass ionomer cements for cementation of orthodontic bands. Isolation, surplus removal and humidity as factors influencing the bond strength between enamel, cement and metal.

作者信息

Liebmann S M, Jost-Brinkmann P G

机构信息

Department of Orthodontics and Dentofacial Orthopedics, University Clinic Charité, Humboldt University, Berlin, Germany.

出版信息

J Orofac Orthop. 1999;60(5):348-60. doi: 10.1007/BF01301247.

Abstract

The aim of this in vitro study was to investigate different light-cured and chemically cured resin-modified glass ionomer cements used for the cementation of orthodontic bands and to analyze various factors influencing the adhesive strength between enamel, cement and stainless steel. Four resin-modified glass ionomers (Fuji Ortho LC/GC, Fuji Duet/GC, Unitek Multi-Cure Glass Ionomer Orthodontic Band Cement/3M Unitek, Vitremer/3M) and 1 compomer (Band-Lok/Reliance) were examined. Flattened and polished bovine teeth embedded in polyurethane resin were used as enamel specimens. Before cementation, 50% of the specimens were moistened with the aerosol of an inhalation device, while the rest were dried with compressed air. Stainless steel cylinders (CrNi 18 10) were perpendicularly bonded onto the polished enamel using a custom-made cementation device and immediately topped with a pressure of 0.25 MPa. The cement was isolated with either Ketac Glaze/ESPE, Fuji Coat/GC, Cacao Butter/GC, Dryfoil/Jalenko or Final Varnish/VOCO, or was left uncoated. Eight minutes after the beginning of mixing, either the surplus cement was removed with a scalpel or surplus removal was simulated with ultrasound. After 24 hours storage in a water bath at 37 degrees C and 1,000 thermocycles the shear bond strength was determined. Significant differences with respect to the shear bond strength were found among the following cements, ranking from highest to lowest: Fuji Duet, Unitek cement > Fuji Ortho LC > Vitremer > Band-Lok. The application of a barrier coating significantly increased the shear bond strength of all cements except Fuji Ortho LC. The light-cured resin Ketac Glaze proved to be the most effective barrier coating. A dry enamel surface increased the bond strength of all investigated cements except Unitek cement. The use of ultrasound led to no significant reduction in shear bond strength in comparison with surplus removal with a scalpel.

摘要

本体外研究的目的是调查用于正畸带环粘结的不同光固化和化学固化树脂改性玻璃离子水门汀,并分析影响牙釉质、水门汀和不锈钢之间粘结强度的各种因素。研究了四种树脂改性玻璃离子水门汀(Fuji Ortho LC/GC、Fuji Duet/GC、Unitek Multi-Cure Glass Ionomer Orthodontic Band Cement/3M Unitek、Vitremer/3M)和一种复合体(Band-Lok/Reliance)。嵌入聚氨酯树脂中的扁平且抛光的牛牙用作牙釉质标本。粘结前,50%的标本用吸入装置的气雾剂湿润,其余标本用压缩空气吹干。使用定制的粘结装置将不锈钢圆柱体(CrNi 18 10)垂直粘结到抛光的牙釉质上,并立即施加0.25 MPa的压力。用水门汀隔离剂Ketac Glaze/ESPE、Fuji Coat/GC、可可脂/GC、Dryfoil/Jalenko或Final Varnish/VOCO隔离水门汀,或不进行涂层处理。混合开始八分钟后,用手术刀去除多余的水门汀,或用超声模拟去除多余水门汀。在37℃的水浴中储存24小时并经过1000次热循环后,测定剪切粘结强度。在以下水门汀之间发现了剪切粘结强度的显著差异,从高到低排序为:Fuji Duet、Unitek水门汀>Fuji Ortho LC>Vitremer>Band-Lok。除Fuji Ortho LC外,屏障涂层的应用显著提高了所有水门汀的剪切粘结强度。光固化树脂Ketac Glaze被证明是最有效的屏障涂层。除Unitek水门汀外,干燥的牙釉质表面增加了所有研究水门汀的粘结强度。与用手术刀去除多余物相比,使用超声导致剪切粘结强度没有显著降低。

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