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带有原子聚焦晶体的电子显微镜中的莫尔条纹

Moiré patterns in electron microscopy with atomic focuser crystals.

作者信息

Cowley JM, Ooi N, Dunin-Borkowski RE

机构信息

Department of Physics and Astronomy, Arizona State University, Tempe, AZ 85287-1504, USA.

出版信息

Acta Crystallogr A. 1999 May 1;55(Pt 3):533-542. doi: 10.1107/s0108767398014950.

Abstract

The periodic array of very fine cross-overs formed at the exit face of a thin 'atomic focuser' crystal, illuminated by a parallel electron beam, may be used to form moiré patterns with a specimen crystal such that the structure of the specimen crystal may be derived with a resolution of better than 0.5 Å. Computer simulations of the moiré pattern formation have been made for the simple idealized case of two parallel gold-like lattices having a 10% difference in lattice constant. Moiré images are shown for the case of a small objective aperture in the viewing electron microscope such that the individual crystal lattices are not resolved and for a larger objective aperture for which the individual crystal lattices are resolved and the intensity is measured at the positions of the atoms of the atomic focuser crystal. The latter case confirms the viability of the scheme for ultra-high-resolution imaging of general specimens by use of a thin-crystal periodic atomic focuser, as previously proposed.

摘要

由平行电子束照射的薄“原子聚焦器”晶体出射面形成的非常精细的交叉点周期性阵列,可用于与样品晶体形成莫尔条纹图案,从而以优于0.5 Å的分辨率得出样品晶体的结构。对于晶格常数相差10%的两个平行类金晶格的简单理想化情况,已进行了莫尔条纹图案形成的计算机模拟。给出了观察电子显微镜中物镜光阑较小时的莫尔图像,此时单个晶格未被分辨;以及物镜光阑较大时的莫尔图像,此时单个晶格被分辨,且在原子聚焦器晶体原子位置处测量强度。后一种情况证实了如先前提出的,使用薄晶体周期性原子聚焦器对一般样品进行超高分辨率成像方案的可行性。

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