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氧化铝基、长石基、白榴石基、云母基和氧化锆基陶瓷的结构可靠性。

Structural reliability of alumina-, feldspar-, leucite-, mica- and zirconia-based ceramics.

作者信息

Tinschert J, Zwez D, Marx R, Anusavice K J

机构信息

Subdepartment for Dental Materials Science and Department of Prosthodontics, University of Aachen, Paulwelsstr. 30, 52074, Aachen, Germany.

出版信息

J Dent. 2000 Sep;28(7):529-35. doi: 10.1016/s0300-5712(00)00030-0.

Abstract

OBJECTIVES

The objective of this study was to test the hypothesis that industrially manufactured ceramic materials, such as Cerec Mark II and Zirconia-TZP, have a smaller range of fracture strength variation and therefore greater structural reliability than laboratory-processed dental ceramic materials.

METHODS

Thirty bar specimens per material were prepared and tested. The four-point bend test was used to determine the flexure strength of all ceramic materials. The fracture stress values were analyzed by Weibull analysis to determine the Weibull modulus values (m) and the 1 and 5% probabilities of failure.

RESULTS

The mean strength and standard deviation values for these ceramics are as follows: (MPa+/-SD) were: Cerec Mark II, 86.3+/-4.3; Dicor, 70.3+/-12.2; In-Ceram Alumina, 429. 3+/-87.2; IPS Empress, 83.9+/-11.3; Vitadur Alpha Core, 131.0+/-9.5; Vitadur Alpha Dentin, 60.7+/-6.8; Vita VMK 68, 82.7+/-10.0; and Zirconia-TZP, 913.0+/-50.2. There was no statistically significant difference among the flexure strength of Cerec Mark II, Dicor, IPS Empress, Vitadur Alpha Dentin, and Vita VMK 68 ceramics (p>0.05). The highest Weibull moduli were associated with Cerec Mark II and Zirconia-TZP ceramics (23.6 and 18.4). Dicor glass-ceramic and In-Ceram Alumina had the lowest m values (5.5 and 5.7), whereas intermediate values were observed for IPS-Empress, Vita VMK 68, Vitadur Alpha Dentin and Vitadur Alpha Core ceramics (8.6, 8.9, 10.0 and 13.0, respectively).

CONCLUSIONS

Except for In-Ceram Alumina, Vitadur Alpha and Zirconia-TZP core ceramics, most of the investigated ceramic materials fabricated under the condition of a dental laboratory were not stronger or more structurally reliable than Vita VMK 68 veneering porcelain. Only Cerec Mark II and Zirconia-TZP specimens, which were prepared from an industrially optimized ceramic material, exhibited m values greater than 18. Hence, we conclude that industrially prepared ceramics are more structurally reliable materials for dental applications although CAD-CAM procedures may induce surface and subsurface flaws that may adversely affect this property.

摘要

目的

本研究的目的是验证以下假设,即工业制造的陶瓷材料,如Cerec Mark II和氧化锆-四方相多晶陶瓷(Zirconia-TZP),其断裂强度变化范围更小,因此比实验室加工的牙科陶瓷材料具有更高的结构可靠性。

方法

每种材料制备30个条形试样并进行测试。采用四点弯曲试验来测定所有陶瓷材料的弯曲强度。通过威布尔分析对断裂应力值进行分析,以确定威布尔模量值(m)以及1%和5%的失效概率。

结果

这些陶瓷的平均强度和标准差如下:(MPa±SD)分别为:Cerec Mark II,86.3±4.3;Dicor,70.3±12.2;In-Ceram氧化铝,429.3±87.2;IPS Empress,83.9±11.3;Vitadur Alpha Core,131.0±9.5;Vitadur Alpha牙本质,60.7±6.8;Vita VMK 68,82.7±10.0;以及氧化锆-四方相多晶陶瓷,913.0±50.2。Cerec Mark II、Dicor、IPS Empress、Vitadur Alpha牙本质和Vita VMK 68陶瓷的弯曲强度之间无统计学显著差异(p>0.05)。最高的威布尔模量与Cerec Mark II和氧化锆-四方相多晶陶瓷相关(分别为23.6和18.4)。Dicor微晶玻璃和In-Ceram氧化铝的m值最低(分别为5.5和5.7),而IPS-Empress、Vita VMK 68、Vitadur Alpha牙本质和Vitadur Alpha Core陶瓷的m值处于中间水平(分别为8.6、8.9、10.0和13.0)。

结论

除了In-Ceram氧化铝、Vitadur Alpha和氧化锆-四方相多晶陶瓷核心材料外,在牙科实验室条件下制备的大多数被研究陶瓷材料并不比Vita VMK 68饰面瓷更强或结构更可靠。只有由工业优化陶瓷材料制备的Cerec Mark II和氧化锆-四方相多晶陶瓷试样的m值大于18。因此,我们得出结论,尽管计算机辅助设计与计算机辅助制造(CAD-CAM)程序可能会产生可能对该性能产生不利影响的表面和亚表面缺陷,但工业制备的陶瓷是更适合牙科应用的结构可靠材料。

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