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[用分光光度法测定消毒剂中的甲醛]

[Measurement of formaldehyde in disinfectant with spectrophotometry].

作者信息

Zhu Y, Wang X, Yang Y, Qi Q

机构信息

Institute of Environmental Health Monitoring, Chinese Academy of Preventive Medicine, Beijing 100021, China.

出版信息

Wei Sheng Yan Jiu. 2001 Jan;30(1):18-9.

Abstract

Formaldehyde in disinfectant was measured by acetylacetone spectrophotometry. The regression equation was linear when the formaldehyde concentration was smaller than 10 micrograms/ml. The detection limit was 0.08 microgram/ml. The accuracy was less than 3.9% and the recovery varied between 100.2%-108.2% for formaldehyde disinfectant with different concentration, which was similar to titrimetry. It was demonstrated that the method was simple, reproducible, sensitive, precise and accurate, making it important for assay of formaldehyde in disinfectant when disturbance caused titrimetry unavailable.

摘要

采用乙酰丙酮分光光度法测定消毒剂中的甲醛。当甲醛浓度小于10微克/毫升时,回归方程呈线性。检测限为0.08微克/毫升。对于不同浓度的甲醛消毒剂,准确度小于3.9%,回收率在100.2% - 108.2%之间,与滴定法相似。结果表明该方法简便、可重复、灵敏、精密且准确,在滴定法因干扰无法使用时,对消毒剂中甲醛的测定具有重要意义。

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