Lidén G, Bergman G
National Institute for Working Life, S-112 79, Stockholm, Sweden.
Ann Occup Hyg. 2001 Apr;45(3):241-52. doi: 10.1016/s0003-4878(00)00052-1.
The weight stability of the sampling cassette of the IOM sampler for inhalable dust was tested in several weighing experiments. The results show that the reliability of repeated weighings was good, but the absorption of water vapour was slow and varied considerably among cassette specimen. The exponential time constant for water absorption was approximately 4 days, and 15-20 days were needed to obtain weight stability. With the help of cassette blanks the imprecision in dust weight could be held below 0.05 mg, if the cassettes were allowed one week's storage in the weighing room before weighing, both before and after sampling. The IOM sampling cassettes seem to consist of a few subsets, each with identical relative weight increase in a weighing room. To keep the variability low it is important that both the blanks and the cassettes used for sampling come from the same subset. Experiments indicate that the conducting plastic of the IOM sampling cassette may be replaced with another kind of plastic with similar electrical conductivity, but whose humidity absorption is 30 times lower. A lid, which is weighed with the cassette, was designed so that the potential dust loss from the cassette proper to the commercial transport clip was eliminated. A flow adapter, which simplifies the measurement of the air flow during personal sampling, was designed.
对可吸入粉尘的IOM采样器采样盒的重量稳定性进行了多次称重实验测试。结果表明,重复称重的可靠性良好,但水汽吸收缓慢,且采样盒样本之间差异很大。水汽吸收的指数时间常数约为4天,需要15 - 20天才能达到重量稳定。借助采样盒空白样本,如果采样前后采样盒在称重室中存放一周后再称重,粉尘重量的不精确性可控制在0.05毫克以下。IOM采样盒似乎由几个子集组成,每个子集在称重室中的相对重量增加相同。为保持低变异性,重要的是空白样本和用于采样的采样盒来自同一子集。实验表明,IOM采样盒的导电塑料可用另一种具有相似电导率但吸湿率低30倍的塑料替代。设计了一种与采样盒一起称重的盖子,以消除采样盒本身向商业运输夹潜在的粉尘损失。设计了一种流量适配器,简化了个人采样期间气流的测量。