Yoshida K, Kamada K, Sawase T, Atsuta M
Department of Fixed Prosthodontics, Nagasaki University School of Dentistry, Nagasaki, Japan.
J Oral Rehabil. 2001 Jan;28(1):14-9. doi: 10.1046/j.1365-2842.2001.00625.x.
The purpose of this study was to evaluate the durability and shear bond strengths of the different combinations of three adhesive primers and three resin cements to a silver-palladium-copper-gold (Ag-Pd-Cu-Au) alloy. The adhesive primers Alloy Primer (AP), Metal PrimerII (MPII) and Metaltite (MT), and the resin cements BistiteII (BRII), Panavia Fluoro Cement (PFC) and Super-Bond C&B (SB) were used. Two sizes of casting alloy disks were either non-primed or primed and cemented with each of the three resin cements. The specimens were stored in a 37 degrees C water bath for 24 h and then immersed alternately in 4 and 60 degrees C water baths for 1 min each for up to 100,000 thermal cycles. Shear mode testing at a crosshead speed of 0.5 mm/min was then performed. The application of MPII or MT was effective for improving the shear bond strength between each of the three resin cements and the Ag-Pd-Cu-Au alloy compared with non-primed specimens. However, when primed with MPII or MT and cemented with SB, the bond strength at 100,000 thermal cycles was significantly lower than that at thermal cycle 0. When primed with AP, the specimens cemented with BRII or PFC showed lower bond strength than non-primed specimens and failed at the metal-resin cement interface at 100,000 thermal cycles. On the other hand, AP was effective in enhancing the shear bond strength of SB to the Ag-Pd-Cu-Au alloy. The five combined uses of an adhesive metal primer and resin cement (combinations of MPII or MT and BRII or PFC and AP and SB) are applicable to the cementation of prosthodontic restorations without complicated surface modification of the noble alloy.
本研究的目的是评估三种粘结底漆与三种树脂水门汀的不同组合对银钯铜金(Ag-Pd-Cu-Au)合金的耐久性和剪切粘结强度。使用了粘结底漆合金底漆(AP)、金属底漆II(MPII)和金属钛(MT),以及树脂水门汀双固化树脂粘结剂II(BRII)、帕纳维亚氟化物水门汀(PFC)和超强粘结剂C&B(SB)。两种尺寸的铸造合金盘要么不进行底漆处理,要么进行底漆处理,并用三种树脂水门汀中的每一种进行粘结。将试样在37℃水浴中储存24小时,然后交替浸入4℃和60℃水浴中各1分钟,进行多达100,000次热循环。然后以0.5mm/min的十字头速度进行剪切模式测试。与未进行底漆处理的试样相比,应用MPII或MT可有效提高三种树脂水门汀与Ag-Pd-Cu-Au合金之间的剪切粘结强度。然而,当用MPII或MT进行底漆处理并与SB粘结时,100,000次热循环后的粘结强度明显低于热循环0时的粘结强度。当用AP进行底漆处理时,用BRII或PFC粘结的试样显示出比未进行底漆处理的试样更低的粘结强度,并在100,000次热循环时在金属-树脂水门汀界面处失效。另一方面,AP可有效提高SB与Ag-Pd-Cu-Au合金的剪切粘结强度。粘结金属底漆和树脂水门汀的五种组合使用方式(MPII或MT与BRII或PFC以及AP与SB的组合)适用于口腔修复体的粘结,而无需对贵金属合金进行复杂的表面改性。