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含硫贵金属底漆对自凝丙烯酸树脂粘结强度的影响。

Effect of Sulfur-Containing Primers for Noble Metals on the Bond Strength of Self-Cured Acrylic Resin.

作者信息

Yoshida Keiichi

机构信息

Clinic of Fixed Prosthodontics, Nagasaki University Hospital, 1-7-1, Sakamoto, Nagasaki 852-8588, Japan.

出版信息

Dent J (Basel). 2017 Jun 20;5(2):22. doi: 10.3390/dj5020022.

DOI:10.3390/dj5020022
PMID:29563428
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5806980/
Abstract

This study investigated the effect of sulfur-containing primers for noble metals on the shear bond strength of self-cured acrylic resin after thermal cycling (TC). Four pure metals (Au, Ag, Cu, and Pd) and type IV Au alloy were either untreated, or treated with one of the five sulfur-containing metal primers (V-Primer, Metaltite, Alloy Primer, Metal Link Primer, and Metal Primer Z). Afterwards, a brass ring was placed on the metal surface and filled with self-cured acrylic resin ( = 10). The bond strengths were measured after 24 h (TC0) and after 2000 thermal cycles at 4-60 °C (TC2000). Three-way ANOVA and Tukey compromise tests were used to analyze the data ( = 0.05). All of the sulfur-containing primers significantly improved the resin bond strength as compared to that of the non-primed group at TC0 regardless of the metal type ( < 0.05). However, at TC2000, the bond strengths between the resin and the five metals significantly decreased with respect to the values obtained at TC0 regardless of the primer ( < 0.05). The sulfur-containing metal primers, except for Metal Link Primer, were found to be more effective for improving the bond strength between the self-cured acrylic resin and Ag as compared to the other three pure metals ( < 0.05). The bond strengths between the resin and Au and type IV Au alloy at TC2000 were the highest ones when Metal Primer Z was used.

摘要

本研究调查了含硫贵金属底漆对热循环(TC)后自凝丙烯酸树脂剪切粘结强度的影响。四种纯金属(金、银、铜和钯)以及IV型金合金,要么未经处理,要么用五种含硫金属底漆(V-Primer、Metaltite、Alloy Primer、Metal Link Primer和Metal Primer Z)之一进行处理。之后,在金属表面放置一个黄铜环,并用自凝丙烯酸树脂填充(n = 10)。在24小时后(TC0)以及在4 - 60°C下进行2000次热循环后(TC2000)测量粘结强度。使用三因素方差分析和Tukey折衷检验来分析数据(α = 0.05)。与未使用底漆的组相比,所有含硫底漆在TC0时均显著提高了树脂粘结强度,无论金属类型如何(p < 0.05)。然而,在TC2000时,无论使用何种底漆,树脂与这五种金属之间的粘结强度相对于在TC0时获得的值均显著降低(p < 0.05)。发现除了Metal Link Primer之外,含硫金属底漆在提高自凝丙烯酸树脂与银之间的粘结强度方面比其他三种纯金属更有效(p < 0.05)。在TC2000时,当使用Metal Primer Z时,树脂与金以及IV型金合金之间的粘结强度是最高的。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/be423d86d2b0/dentistry-05-00022-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/9e0fabe18884/dentistry-05-00022-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/2a7d02abe0dc/dentistry-05-00022-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/03e54e21ed71/dentistry-05-00022-g003a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/9879c0b72cbc/dentistry-05-00022-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/f7248256c714/dentistry-05-00022-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/be423d86d2b0/dentistry-05-00022-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/9e0fabe18884/dentistry-05-00022-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/2a7d02abe0dc/dentistry-05-00022-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/03e54e21ed71/dentistry-05-00022-g003a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/9879c0b72cbc/dentistry-05-00022-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/f7248256c714/dentistry-05-00022-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58ea/5806980/be423d86d2b0/dentistry-05-00022-g006.jpg

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本文引用的文献

1
Effect of metal primers and tarnish treatment on bonding between dental alloys and veneer resin.金属底漆和防变色处理对牙科合金与贴面树脂之间粘结的影响。
J Adv Prosthodont. 2015 Oct;7(5):392-9. doi: 10.4047/jap.2015.7.5.392. Epub 2015 Oct 28.
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Thermal cycling for restorative materials: does a standardized protocol exist in laboratory testing? A literature review.修复材料的热循环:实验室测试中是否存在标准化方案?文献综述。
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A review of the developments of multi-purpose primers and adhesives comprising novel dithiooctanoate monomers and phosphonic acid monomers.
综述了包含新型二硫辛酯单体和膦酸单体的多用途引物和胶粘剂的发展。
Dent Mater J. 2012 Feb 3;31(1):1-25. doi: 10.4012/dmj.2011-139. Epub 2012 Jan 21.
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Design of a metal primer containing a dithiooctanoate monomer and a phosphonic acid monomer for bonding of prosthetic light-curing resin composite to gold, dental precious and non-precious metal alloys.用于将义齿光固化树脂复合材料与金、牙科贵金属和非贵金属合金粘结的含二硫代辛二酸单体和膦酸单体的金属底涂剂的设计。
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Effects of metal primers on bonding of adhesive resin cement to noble alloys for porcelain fusing.金属底涂剂对贵金属合金烤瓷焊接用黏结树脂水门汀黏结性能的影响。
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Effects of primers containing sulfur and phosphate monomers on bonding type IV gold alloy.含硫和磷单体的底漆对IV型金合金粘结的影响。
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Water durability of resin bond to pure gold treated with various adhesion promoting thiirane monomers.用各种促进粘合的硫杂环丙烷单体处理后,树脂与纯金之间的水耐久性。
Dent Mater J. 2007 Jan;26(1):29-37. doi: 10.4012/dmj.26.29.
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Raman and IR studies on adsorption behavior of adhesive monomers in a metal primer for Au, Ag, Cu, and Cr surfaces.拉曼光谱和红外光谱对用于金、银、铜和铬表面的金属底漆中胶粘剂单体吸附行为的研究。
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Effect of ceramic surface treatment on tensile bond strength to a resin cement.陶瓷表面处理对与树脂水门汀拉伸粘结强度的影响。
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Tensile bond strength of resin-modified glass-ionomer cement to microabraded and silica-coated or tin-plated high noble ceramic alloy.树脂改性玻璃离子水门汀与微磨损及二氧化硅涂层或镀锡高贵金属陶瓷合金的拉伸粘结强度。
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