Yoshida Keiichi
Clinic of Fixed Prosthodontics, Nagasaki University Hospital, 1-7-1, Sakamoto, Nagasaki 852-8588, Japan.
Dent J (Basel). 2017 Jun 20;5(2):22. doi: 10.3390/dj5020022.
This study investigated the effect of sulfur-containing primers for noble metals on the shear bond strength of self-cured acrylic resin after thermal cycling (TC). Four pure metals (Au, Ag, Cu, and Pd) and type IV Au alloy were either untreated, or treated with one of the five sulfur-containing metal primers (V-Primer, Metaltite, Alloy Primer, Metal Link Primer, and Metal Primer Z). Afterwards, a brass ring was placed on the metal surface and filled with self-cured acrylic resin ( = 10). The bond strengths were measured after 24 h (TC0) and after 2000 thermal cycles at 4-60 °C (TC2000). Three-way ANOVA and Tukey compromise tests were used to analyze the data ( = 0.05). All of the sulfur-containing primers significantly improved the resin bond strength as compared to that of the non-primed group at TC0 regardless of the metal type ( < 0.05). However, at TC2000, the bond strengths between the resin and the five metals significantly decreased with respect to the values obtained at TC0 regardless of the primer ( < 0.05). The sulfur-containing metal primers, except for Metal Link Primer, were found to be more effective for improving the bond strength between the self-cured acrylic resin and Ag as compared to the other three pure metals ( < 0.05). The bond strengths between the resin and Au and type IV Au alloy at TC2000 were the highest ones when Metal Primer Z was used.
本研究调查了含硫贵金属底漆对热循环(TC)后自凝丙烯酸树脂剪切粘结强度的影响。四种纯金属(金、银、铜和钯)以及IV型金合金,要么未经处理,要么用五种含硫金属底漆(V-Primer、Metaltite、Alloy Primer、Metal Link Primer和Metal Primer Z)之一进行处理。之后,在金属表面放置一个黄铜环,并用自凝丙烯酸树脂填充(n = 10)。在24小时后(TC0)以及在4 - 60°C下进行2000次热循环后(TC2000)测量粘结强度。使用三因素方差分析和Tukey折衷检验来分析数据(α = 0.05)。与未使用底漆的组相比,所有含硫底漆在TC0时均显著提高了树脂粘结强度,无论金属类型如何(p < 0.05)。然而,在TC2000时,无论使用何种底漆,树脂与这五种金属之间的粘结强度相对于在TC0时获得的值均显著降低(p < 0.05)。发现除了Metal Link Primer之外,含硫金属底漆在提高自凝丙烯酸树脂与银之间的粘结强度方面比其他三种纯金属更有效(p < 0.05)。在TC2000时,当使用Metal Primer Z时,树脂与金以及IV型金合金之间的粘结强度是最高的。