Smallfield B M, van Klink J W, Perry N B, Dodds K G
New Zealand Institute for Crop and Food Research Ltd., Invermay Agriculture Centre, Mosgiel, New Zealand.
J Agric Food Chem. 2001 Jan;49(1):118-23. doi: 10.1021/jf001024s.
Crushing intensity and distillation time were evaluated for their effects on the oil yield and composition of steam-distilled essential oil from fruits of Coriandrum sativum var. microcarpum L. A comparison of oils produced by laboratory- and pilot-scale stills showed that the two still types gave comparable yields and oil composition. The laboratory still was then used to compare oil yields and compositions from fruits crushed at three different intensities, at intervals during a distillation period of 60 min. Both crushing intensity and distillation time had significant (P< 0.05) effects on the yield and composition of the oil. The maximum oil yield was less from the light-crushed fruits, but the rate of oil recovery was significantly P < 0.05) higher. From the light-crushed fruits, 95% of the maximum yield was extracted in 22.5 min compared with 32 and 39 min for the standard and heavy-crushed fruits, respectively. The effect of crushing intensity on oil composition was most pronounced on the low-boiling-point a-pinene and on the higher-boiling-point geranyl acetate. Crushing had little effect on linalool content, but distillation time could be manipulated to alter the linalool content of the oil.
研究了粉碎强度和蒸馏时间对小茴香果实水蒸气蒸馏精油得率及成分的影响。对实验室规模和中试规模蒸馏器所产精油的比较表明,两种蒸馏器的得率和精油成分相当。随后使用实验室蒸馏器比较了在60分钟蒸馏期间,以三种不同强度粉碎的果实的精油得率和成分。粉碎强度和蒸馏时间对精油的得率和成分均有显著(P<0.05)影响。轻度粉碎的果实精油得率最高,但精油回收率显著(P<0.05)更高。对于轻度粉碎的果实,在22.5分钟内提取了最大得率的95%,而标准粉碎和重度粉碎的果实分别需要32分钟和39分钟。粉碎强度对精油成分的影响在低沸点的α-蒎烯和高沸点的乙酸香叶酯上最为明显。粉碎对芳樟醇含量影响不大,但可通过控制蒸馏时间来改变精油中芳樟醇的含量。