Lin S N, Horning E C
J Chromatogr. 1975 Oct 29;112:465-82. doi: 10.1016/s0021-9673(00)99977-1.
A new gas chromatographic procedure was developed for the concurrent analysis of mixtures of long-chain acids (as methyl esters), cholesterol (as the trimethylsilyl ether) and the tocopherols (as trimethylsilyl ethers). This method was used in a study of free fatty acids and alpha-tocopherol in the plasma of normal subjects and stroke patients. The chromatographic separation was based upon the use of thermostable glass open tubular capillary columns prepared with Silanox (procedure of Lin, Pfaffenberger and Horning) and a new polar liquid phase (Schwartz-Mathews polyphenyl ether sulfone phase). The German-Horning injection system was used in a modified gas chromatograph.
开发了一种新的气相色谱法，用于同时分析长链酸（作为甲酯）、胆固醇（作为三甲基硅醚）和生育酚（作为三甲基硅醚）的混合物。该方法用于研究正常受试者和中风患者血浆中的游离脂肪酸和α-生育酚。色谱分离基于使用用Silanox制备的热稳定玻璃开管毛细管柱（Lin、Pfaffenberger和Horning的方法）和一种新的极性液相（Schwartz-Mathews聚苯醚砜相）。在改良的气相色谱仪中使用了German-Horning进样系统。
